C₂₅H₁₈BrNO₆S

Base Information

• Chemical Name: C₂₅H₁₈BrNO₆S
• CAS No.: 1313833-06-5
• Molecular Formula: C₂₅H₁₈BrNO₆S
• Molecular Weight: 540.391
• Mol file: 1313833-06-5.mol

Synonyms:

Chemical Property of C₂₅H₁₈BrNO₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₁₈BrNO₆S

There total 4 articles about C₂₅H₁₈BrNO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 5-hydroxy-2-methyl-benzofuran-3-carboxylate (7287-40-3) → C25H18BrNO6S (1313833-06-5)

Guidance literature:

Multi-step reaction with 4 steps

1: bromine / 1,4-dioxane / 0.5 h

2: trifluoroacetic acid / Reflux

3: piperidine / ethanol / 24 h / 20 °C

4: sulfuric acid; water / Reflux

With piperidine; sulfuric acid; water; bromine; trifluoroacetic acid; In 1,4-dioxane; ethanol; 2: Duff reaction;

DOI:10.1007/s10593-011-0886-x

Reference yield:

ethyl 5-bromo-4-hydroxy-2-methylbenzofuran-3-carboxylate (7287-41-4) → C25H18BrNO6S (1313833-06-5)

Guidance literature:

Multi-step reaction with 3 steps

1: trifluoroacetic acid / Reflux

2: piperidine / ethanol / 24 h / 20 °C

3: sulfuric acid; water / Reflux

With piperidine; sulfuric acid; water; trifluoroacetic acid; In ethanol; 1: Duff reaction;

DOI:10.1007/s10593-011-0886-x

Reference yield:

C13H11BrO5 (308295-26-3) + 2-(4-(4-methoxyphenyl)thiazol-2-yl)acetonitrile (301235-86-9) → C25H18BrNO6S (1313833-06-5)

Guidance literature:

Multi-step reaction with 2 steps

1: piperidine / ethanol / 24 h / 20 °C

2: sulfuric acid; water / Reflux

With piperidine; sulfuric acid; water; In ethanol;

DOI:10.1007/s10593-011-0886-x

upstream raw materials:

ethyl 5-bromo-4-hydroxy-2-methylbenzofuran-3-carboxylate

C₁₃H₁₁BrO₅

2-(4-(4-methoxyphenyl)thiazol-2-yl)acetonitrile

ethyl 5-hydroxy-2-methyl-benzofuran-3-carboxylate

Refernces