C₁₃H₁₄ClNO

Base Information

Chemical Name:C₁₃H₁₄ClNO
CAS No.:1413938-96-1
Molecular Formula:C₁₃H₁₄ClNO
Molecular Weight:235.713
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₄ClNO

Chemical Property:

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Technology Process of C₁₃H₁₄ClNO

There total 2 articles about C₁₃H₁₄ClNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426828-61-6
C₁₅H₁₈ClNO

: 1413938-96-1
C₁₃H₁₄ClNO

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 40 ℃; Inert atmosphere;
DOI:10.1021/ml300262e

Reference yield:

: 51230-92-3
2-(4-chlorophenyl)pent-4-enoic acid

: 1413938-96-1
C₁₃H₁₄ClNO

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; 2-chloro-1-methyl-pyridinium iodide / dichloromethane / 20 °C

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 40 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ml300262e

Reference yield:

: 1413938-96-1
C₁₃H₁₄ClNO

: 1413938-74-5
3-(4-chlorophenyl)-2,3,4,7-tetrahydro-1H-azepine monoformate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / Cooling with ice; Reflux

2: carbonochloridic acid 1-chloro-ethyl ester / toluene / Cooling with ice; Reflux

With lithium aluminium tetrahydride; carbonochloridic acid 1-chloro-ethyl ester; In tetrahydrofuran; toluene;
DOI:10.1021/ml300262e