(2-((3-(2,4-Bis(benzyloxy)-3,5,6-trifluorobenzyl-oxy)phenoxy)methyl)-4,6-difluorobenzene-1,-3,5-triyl)tris(oxy)tris(methylene)tribenzene

Base Information

• Chemical Name: (2-((3-(2,4-Bis(benzyloxy)-3,5,6-trifluorobenzyl-oxy)phenoxy)methyl)-4,6-difluorobenzene-1,-3,5-triyl)tris(oxy)tris(methylene)tribenzene
• CAS No.: 1612762-81-8
• Molecular Formula: C₅₅H₄₃F₅O₇
• Molecular Weight: 910.934
• Mol file: 1612762-81-8.mol

Synonyms:

Chemical Property of (2-((3-(2,4-Bis(benzyloxy)-3,5,6-trifluorobenzyl-oxy)phenoxy)methyl)-4,6-difluorobenzene-1,-3,5-triyl)tris(oxy)tris(methylene)tribenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-((3-(2,4-Bis(benzyloxy)-3,5,6-trifluorobenzyl-oxy)phenoxy)methyl)-4,6-difluorobenzene-1,-3,5-triyl)tris(oxy)tris(methylene)tribenzene

There total 3 articles about (2-((3-(2,4-Bis(benzyloxy)-3,5,6-trifluorobenzyl-oxy)phenoxy)methyl)-4,6-difluorobenzene-1,-3,5-triyl)tris(oxy)tris(methylene)tribenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.2%

3,5-Bis[(pentafluorobenzyl)oxy]benzene (1612762-78-3) + benzyl alcohol (100-51-6,185532-71-2) → (2-((3-(2,4-Bis(benzyloxy)-3,5,6-trifluorobenzyl-oxy)phenoxy)methyl)-4,6-difluorobenzene-1,-3,5-triyl)tris(oxy)tris(methylene)tribenzene (1612762-81-8)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetonitrile; for 24h; Reflux;

DOI:10.1002/pola.27078

Reference yield:

recorcinol (108-46-3) → (2-((3-(2,4-Bis(benzyloxy)-3,5,6-trifluorobenzyl-oxy)phenoxy)methyl)-4,6-difluorobenzene-1,-3,5-triyl)tris(oxy)tris(methylene)tribenzene (1612762-81-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 18-crown-6 ether; potassium carbonate / acetone / 96 h / 20 °C / Inert atmosphere

2: 18-crown-6 ether; potassium carbonate / acetonitrile / 24 h / Reflux

With 18-crown-6 ether; potassium carbonate; In acetone; acetonitrile;

DOI:10.1002/pola.27078

Reference yield:

(bromomethyl)pentafluorobenzene (1765-40-8) → (2-((3-(2,4-Bis(benzyloxy)-3,5,6-trifluorobenzyl-oxy)phenoxy)methyl)-4,6-difluorobenzene-1,-3,5-triyl)tris(oxy)tris(methylene)tribenzene (1612762-81-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 18-crown-6 ether; potassium carbonate / acetone / 96 h / 20 °C / Inert atmosphere

2: 18-crown-6 ether; potassium carbonate / acetonitrile / 24 h / Reflux

With 18-crown-6 ether; potassium carbonate; In acetone; acetonitrile;

DOI:10.1002/pola.27078

upstream raw materials:

3,5-Bis[(pentafluorobenzyl)oxy]benzene

benzyl alcohol

recorcinol

(bromomethyl)pentafluorobenzene