Technology Process of C21H19F2N5O5
There total 10 articles about C21H19F2N5O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide;
In
tetrahydrofuran; methanol; water;
at 35 ℃;
DOI:10.1039/c2md20187a
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 180 °C / Microwave irradiation
2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate
3.1: pyridine / dichloromethane
4.1: hydrazine hydrate / ethanol
5.1: DMA
5.2: 60 °C
6.1: lithium hydroxide / tetrahydrofuran; water; methanol / 35 °C
With
pyridine; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; hydrazine hydrate; triphenylphosphine; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate;
1.1: |Mitsunobu Displacement;
DOI:10.1039/c2md20187a
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 180 °C / Microwave irradiation
2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate
3.1: pyridine / dichloromethane
4.1: hydrazine hydrate / ethanol
5.1: DMA
5.2: 60 °C
6.1: lithium hydroxide / tetrahydrofuran; water; methanol / 35 °C
With
pyridine; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; hydrazine hydrate; triphenylphosphine; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate;
1.1: |Mitsunobu Displacement;
DOI:10.1039/c2md20187a