1,4-bis-(5-perfluorophenylthien-2-yl)-2,5-dioctyloxybenzene

Base Information

Chemical Name:1,4-bis-(5-perfluorophenylthien-2-yl)-2,5-dioctyloxybenzene
CAS No.:1443616-41-8
Molecular Formula:C₄₂H₄₀F₁₀O₂S₂
Molecular Weight:830.894
Hs Code.:

Synonyms:

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Chemical Property of 1,4-bis-(5-perfluorophenylthien-2-yl)-2,5-dioctyloxybenzene

Chemical Property:

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Technology Process of 1,4-bis-(5-perfluorophenylthien-2-yl)-2,5-dioctyloxybenzene

There total 5 articles about 1,4-bis-(5-perfluorophenylthien-2-yl)-2,5-dioctyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 344-04-7
bromopentafluorobenzene

: 1443616-41-8
1,4-bis-(5-perfluorophenylthien-2-yl)-2,5-dioctyloxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 72 h / 80 °C / Inert atmosphere

3.2: 2 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: |Stille Cross Coupling / 3.1: |Stille Cross Coupling;
DOI:10.1002/chem.201203869

Reference yield:

: 67399-94-4
1,4-bis(octyloxy)benzene

: 1443616-41-8
1,4-bis-(5-perfluorophenylthien-2-yl)-2,5-dioctyloxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium iodate; iodine; sulfuric acid / acetic acid; water / 48 h / Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 72 h / 80 °C / Inert atmosphere

2.2: 2 h

With potassium iodate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; iodine; In tetrahydrofuran; water; acetic acid; N,N-dimethyl-formamide; 2.1: |Stille Cross Coupling;
DOI:10.1002/chem.201203869

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 1443616-41-8
1,4-bis-(5-perfluorophenylthien-2-yl)-2,5-dioctyloxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol / 1 h / 20 °C

1.2: 24 h / Reflux

2.1: potassium iodate; iodine; sulfuric acid / acetic acid; water / 48 h / Reflux

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 72 h / 80 °C / Inert atmosphere

3.2: 2 h

With potassium iodate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; iodine; potassium hydroxide; In tetrahydrofuran; ethanol; water; acetic acid; N,N-dimethyl-formamide; 3.1: |Stille Cross Coupling;
DOI:10.1002/chem.201203869