1-Methyl-2,3-dihydro-1H-cyclopenta[b]quinoxaline

Base Information

Chemical Name:1-Methyl-2,3-dihydro-1H-cyclopenta[b]quinoxaline
CAS No.:26629-21-0
Molecular Formula:C₁₂H₁₂N₂
Molecular Weight:184.241
Hs Code.:
NSC Number:109966
DSSTox Substance ID:DTXSID80296585

Synonyms:1-Methyl-2,3-dihydro-1H-cyclopenta[b]quinoxaline;26629-21-0;3-methyl-2,3-dihydro-1H-cyclopenta[b]quinoxaline;NSC109966;DTXSID80296585;NVQOTQXRJHBSOP-UHFFFAOYSA-N;NSC-109966;2,3-Dihydro-1H-1-methylcyclopenta[b]quinoxaline;2,3-Dihydro-(1H)1-methylcyclopenta[b]quinoxaline;1-Methyl-2,3-dihydro-1H-cyclopenta[b]quinoxaline #

Suppliers and Price of 1-Methyl-2,3-dihydro-1H-cyclopenta[b]quinoxaline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-Methyl-2,3-dihydro-1H-cyclopenta[b]quinoxaline

Chemical Property:

Vapor Pressure:0.00061mmHg at 25°C
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:184.100048391
Heavy Atom Count:14
Complexity:216

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1CCC2=NC3=CC=CC=C3N=C12

Technology Process of 1-Methyl-2,3-dihydro-1H-cyclopenta[b]quinoxaline

There total 5 articles about 1-Methyl-2,3-dihydro-1H-cyclopenta[b]quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 80-71-7
2-hydroxy-3-methylcyclopent-2-en-1-one

: 95-54-5
1,2-diamino-benzene

: 26629-21-0
2,3-dihydro-1H-1-methylcyclopenta(b)quinoxaline

Guidance literature:: In ethanol; at 80 ℃;
DOI:10.1002/cssc.201702100

Reference yield:

: 67-47-0
5-hydroxymethyl-2-furfuraldehyde

: 26629-21-0
2,3-dihydro-1H-1-methylcyclopenta(b)quinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; [Ir(η⁵-Cp*)(2,2'-dipyridylamine)Cl]Cl / water / 2 h / 120 °C / 7500.75 Torr

2: potassium tert-butylate / tetrahydrofuran / 0.08 h / 60 °C

3: ethanol / 80 °C

With [Ir(η⁵-Cp*)(2,2'-dipyridylamine)Cl]Cl; potassium tert-butylate; hydrogen; In tetrahydrofuran; ethanol; water; 1: |Aldol Condensation / 2: |Aldol Condensation;
DOI:10.1002/cssc.201702100

Reference yield:

: 65313-46-4
1-hydroxyl-2,5-hexanedione

: 26629-21-0
2,3-dihydro-1H-1-methylcyclopenta(b)quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 0.08 h / 60 °C

2: ethanol / 80 °C

With potassium tert-butylate; In tetrahydrofuran; ethanol; 1: |Aldol Condensation;
DOI:10.1002/cssc.201702100