N--4-methoxybenzolsulfonamid

Base Information

Chemical Name:N--4-methoxybenzolsulfonamid
CAS No.:84274-87-3
Molecular Formula:C₁₀H₁₅N₃O₃S
Molecular Weight:257.313
Hs Code.:

N-<Amino(dimethylamino)methylen>-4-methoxybenzolsulfonamid

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Suppliers and Price of N--4-methoxybenzolsulfonamid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N--4-methoxybenzolsulfonamid

Chemical Property:

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Technology Process of N--4-methoxybenzolsulfonamid

There total 5 articles about N--4-methoxybenzolsulfonamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 13750-34-0
N--p-toluolsulfonamid

: 105-45-3
acetoacetic acid methyl ester

: 24762-04-7
2-Diazo-3-oxo-butyric acid methyl ester

: 84274-87-3
N--4-methoxybenzolsulfonamid

Guidance literature:: With triethylamine; In acetonitrile; for 3h; Product distribution; Ambient temperature; other N',N'-disubstituted N-arenesulfonamides investigated;

Reference yield: 43.0%

: 84274-74-8
N--4-methoxybenzolsulfonamid

: 24762-04-7
2-Diazo-3-oxo-butyric acid methyl ester

: 84274-87-3
N--4-methoxybenzolsulfonamid

Guidance literature:: With acetoacetic acid methyl ester; triethylamine; In acetonitrile; for 3h; Ambient temperature;

Reference yield:

: 1129-26-6
4-methoxybenzene sulfonamide

: 84274-87-3
N--4-methoxybenzolsulfonamid

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / benzene / 2 h / Heating

2: 75 percent / N₂H₄*H₂O / ethanol / 1 h / Ambient temperature

3: 46 percent / isoamylnitrite / CHCl₃; acetic acid / 2 h / Ambient temperature

4: 97 percent / CH₃COCH₂COOCH₃, N(C₂H₅)3 / acetonitrile / 3 h / Ambient temperature

With hydrazine hydrate; acetoacetic acid methyl ester; triethylamine; isopentyl nitrite; In ethanol; chloroform; acetic acid; acetonitrile; benzene;