Benzyl-4,6-O-benzyliden-2-chlor-2,3-didesoxy-3-(2',4'-dinitroanilino)-α-D-altropyranosid

Base Information

Chemical Name:Benzyl-4,6-O-benzyliden-2-chlor-2,3-didesoxy-3-(2',4'-dinitroanilino)-α-D-altropyranosid
CAS No.:81429-65-4
Molecular Formula:C₂₆H₂₄ClN₃O₈
Molecular Weight:541.945
Hs Code.:

Synonyms:

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Chemical Property of Benzyl-4,6-O-benzyliden-2-chlor-2,3-didesoxy-3-(2',4'-dinitroanilino)-α-D-altropyranosid

Chemical Property:

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Technology Process of Benzyl-4,6-O-benzyliden-2-chlor-2,3-didesoxy-3-(2',4'-dinitroanilino)-α-D-altropyranosid

There total 3 articles about Benzyl-4,6-O-benzyliden-2-chlor-2,3-didesoxy-3-(2',4'-dinitroanilino)-α-D-altropyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 73793-28-9
Benzyl-4,6-O-benzyliden-2,3-didesoxy-N-(2',4'-dinitrophenyl)-2,3-epimino-α-D-allopyranosid

: 81429-65-4
Benzyl-4,6-O-benzyliden-2-chlor-2,3-didesoxy-3-(2',4'-dinitroanilino)-α-D-altropyranosid

: 81429-66-5
Benzyl-4,6-O-benzyliden-3-chlor-2,3-didesoxy-2-(2',4'-dinitroanilino)-α-D-glucopyranosid

Guidance literature:: With ammonium chloride; sodium chloride; In N,N-dimethyl-formamide; for 3h; Heating;

Reference yield:

: 13343-65-2
Benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methanesulfonyl-α-D-glucopyranoside

: 81429-65-4
Benzyl-4,6-O-benzyliden-2-chlor-2,3-didesoxy-3-(2',4'-dinitroanilino)-α-D-altropyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / sodium isopropylate / dioxane / 12 h / Heating

2: 72 percent / NaHCO₃ / dimethylformamide / 60 h

3: 37 percent / NaCl, NH₄Cl / dimethylformamide / 3 h / Heating

With sodium isopropylate; sodium hydrogencarbonate; ammonium chloride; sodium chloride; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 73793-32-5
benzyl 4,6-O-benzylidene-2,3-dideoxy-2,3-epimino-α-D-allopyranoside

: 81429-65-4
Benzyl-4,6-O-benzyliden-2-chlor-2,3-didesoxy-3-(2',4'-dinitroanilino)-α-D-altropyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / NaHCO₃ / dimethylformamide / 60 h

2: 37 percent / NaCl, NH₄Cl / dimethylformamide / 3 h / Heating

With sodium hydrogencarbonate; ammonium chloride; sodium chloride; In N,N-dimethyl-formamide;