<9-Phenyl-fluorenyl-(1)>-essigsaeure

Base Information

• Chemical Name: <9-Phenyl-fluorenyl-(1)>-essigsaeure
• CAS No.: 18554-18-2
• Molecular Formula: C₂₁H₁₆O₂
• Molecular Weight: 300.357

Synonyms:

Chemical Property of <9-Phenyl-fluorenyl-(1)>-essigsaeure

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Technology Process of <9-Phenyl-fluorenyl-(1)>-essigsaeure

There total 1 articles about <9-Phenyl-fluorenyl-(1)>-essigsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<9-Phenyl-fluorenyl-(9)>-carbonyldiazomethan (18554-45-5) → <9-Phenyl-fluorenyl-(1)>-essigsaeure (18554-18-2)

Guidance literature:

Multistep reaction; (i) 4-ethyl-morpholine, hexan-1-ol (heating), (ii) KOH;

DOI:10.1021/jo01260a032

Reference yield:

<9-Phenyl-fluorenyl-(1)>-essigsaeure (18554-18-2) → 1-methyl-9-phenyl-9H-fluorene (18554-50-2)

Guidance literature:

With isoquinoline; copper; at 225 - 235 ℃;

DOI:10.1021/jo01260a032

upstream raw materials:

<9-Phenyl-fluorenyl-(9)>-carbonyldiazomethan

Downstream raw materials:

1-methyl-9-phenyl-9H-fluorene

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