Technology Process of N1,N9-dipropyl-N1,N5,N9-tris(mesitylenesulfonyl)homospermidine
There total 5 articles about N1,N9-dipropyl-N1,N5,N9-tris(mesitylenesulfonyl)homospermidine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 31 percent / 1 N aq. NaOH / CH2Cl2 / Ambient temperature
2: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) DMF, RT, 12 h
With
sodium hydroxide; sodium hydride;
In
dichloromethane;
DOI:10.1021/jm960849j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) DMF, 60 deg C, overnight
2: 76 percent / hydrazine monohydrate / ethanol / 24 h / 65 °C
3: 31 percent / 1 N aq. NaOH / CH2Cl2 / Ambient temperature
4: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) DMF, RT, 12 h
With
sodium hydroxide; sodium hydride; hydrazine hydrate;
In
ethanol; dichloromethane;
DOI:10.1021/jm960849j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 31 percent / 1 N aq. NaOH / CH2Cl2 / Ambient temperature
2: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) DMF, RT, 12 h
With
sodium hydroxide; sodium hydride;
In
dichloromethane;
DOI:10.1021/jm960849j
