Technology Process of (3S,4S)-3,4-dibenzoyloxy-1-tert-butoxycarbonylpyrrolidine
There total 3 articles about (3S,4S)-3,4-dibenzoyloxy-1-tert-butoxycarbonylpyrrolidine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 96 percent / Na2CO3 / CH2Cl2; H2O / 2 h / Ambient temperature
2: 1.) AcOH, H2, 2.) aq. KOH / 1.) 20percent Pd(OH)2/C / 1.) 4 atm, 24 h, 2.) methanol
3: CHCl3
With
potassium hydroxide; hydrogen; sodium carbonate; acetic acid;
palladium dihydroxide;
In
dichloromethane; chloroform; water;
DOI:10.1248/cpb.39.2219
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) AcOH, H2, 2.) aq. KOH / 1.) 20percent Pd(OH)2/C / 1.) 4 atm, 24 h, 2.) methanol
2: CHCl3
With
potassium hydroxide; hydrogen; acetic acid;
palladium dihydroxide;
In
chloroform;
DOI:10.1248/cpb.39.2219
