o-nitrobenzylidene du benzoylacetate d'ethyle

Base Information

Chemical Name:o-nitrobenzylidene du benzoylacetate d'ethyle
CAS No.:125105-18-2
Molecular Formula:C₁₈H₁₅NO₅
Molecular Weight:325.321
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-nitrobenzylidene du benzoylacetate d'ethyle

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Technology Process of o-nitrobenzylidene du benzoylacetate d'ethyle

There total 3 articles about o-nitrobenzylidene du benzoylacetate d'ethyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 64967-44-8
(Z)-ethyl 3-acetyloxy-3-phenyl-2-propenoate

: 552-89-6
2-nitro-benzaldehyde

: 125105-18-2
o-nitrobenzylidene du benzoylacetate d'ethyle

Guidance literature:: With Porcine Pancreas Lipase; In water; tert-butyl alcohol; Enzymatic reaction;
DOI:10.1002/chem.201901491

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 125105-18-2
o-nitrobenzylidene du benzoylacetate d'ethyle

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 0.25 h / 120 °C

2: Porcine Pancreas Lipase / tert-butyl alcohol; water / Enzymatic reaction

With pyridine; Porcine Pancreas Lipase; In water; tert-butyl alcohol; 2: |Knoevenagel Condensation;
DOI:10.1002/chem.201901491