4-Bis-2-t-butyl-3-phenyl-1,2,4-oxadiazolidin-5-one

Base Information

Chemical Name:4-Bis-2-t-butyl-3-phenyl-1,2,4-oxadiazolidin-5-one
CAS No.:98834-83-4
Molecular Formula:C₂₅H₂₆N₂O₂S₂
Molecular Weight:450.626
Hs Code.:

4-Bis<phenylthiomethyl>-2-t-butyl-3-phenyl-1,2,4-oxadiazolidin-5-one

Synonyms:

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Chemical Property of 4-Bis-2-t-butyl-3-phenyl-1,2,4-oxadiazolidin-5-one

Chemical Property:

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Technology Process of 4-Bis-2-t-butyl-3-phenyl-1,2,4-oxadiazolidin-5-one

There total 4 articles about 4-Bis-2-t-butyl-3-phenyl-1,2,4-oxadiazolidin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 3376-24-7,68315-30-0
N-tert-butyl-α-phenylnitrone

: 98834-75-4
Bismethyl isocyanate

: 98834-83-4
4-Bis-2-t-butyl-3-phenyl-1,2,4-oxadiazolidin-5-one

Guidance literature:: In benzene; for 16h; Heating;
DOI:10.1055/s-1985-31175

Reference yield:

: 1914-64-3
Bisacetic acid

: 98834-83-4
4-Bis-2-t-butyl-3-phenyl-1,2,4-oxadiazolidin-5-one

Guidance literature:: Multi-step reaction with 4 steps

1: Thionyl chloride / hexane; methanol / 2 h / 60 - 70 °C

2: NaN₃ / H₂O / 1 h / 0 °C

3: Cu powder / benzene; diethyl ether / 1 h / Heating

4: 74 percent / benzene / 16 h / Heating

With thionyl chloride; sodium azide; copper; In methanol; diethyl ether; hexane; water; benzene;
DOI:10.1055/s-1985-31175

Reference yield:

: 98834-76-5
Bis-phenylsulfanyl-acetyl chloride

: 98834-83-4
4-Bis-2-t-butyl-3-phenyl-1,2,4-oxadiazolidin-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / H₂O / 1 h / 0 °C

2: Cu powder / benzene; diethyl ether / 1 h / Heating

3: 74 percent / benzene / 16 h / Heating

With sodium azide; copper; In diethyl ether; water; benzene;
DOI:10.1055/s-1985-31175