(E)-(2S,6R)-4-Benzenesulfonyl-2-{(4R,5S,6R)-6-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-6,9-dimethyl-dec-7-en-3-ol

Base Information

Chemical Name:(E)-(2S,6R)-4-Benzenesulfonyl-2-{(4R,5S,6R)-6-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-6,9-dimethyl-dec-7-en-3-ol
CAS No.:122213-34-7
Molecular Formula:C₄₄H₆₄O₆SSi
Molecular Weight:749.14
Hs Code.:

(E)-(2S,6R)-4-Benzenesulfonyl-2-{(4R,5S,6R)-6-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-6,9-dimethyl-dec-7-en-3-ol

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Chemical Property of (E)-(2S,6R)-4-Benzenesulfonyl-2-{(4R,5S,6R)-6-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-6,9-dimethyl-dec-7-en-3-ol

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Technology Process of (E)-(2S,6R)-4-Benzenesulfonyl-2-{(4R,5S,6R)-6-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-6,9-dimethyl-dec-7-en-3-ol

There total 9 articles about (E)-(2S,6R)-4-Benzenesulfonyl-2-{(4R,5S,6R)-6-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-6,9-dimethyl-dec-7-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122213-32-5
(E)-(R)-7-Bromo-2,5-dimethyl-hept-3-ene

: 122213-34-7,122292-27-7,122292-28-8,122292-29-9
(E)-(2S,6R)-4-Benzenesulfonyl-2-{(4R,5S,6R)-6-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-6,9-dimethyl-dec-7-en-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / dimethylformamide / Ambient temperature

2: 1.) n-BuLi / 1.) THF, -78 deg C, 45 min, 2.) a) THF, -78 deg C, 50 min, b) 0 deg C, 30 min

With n-butyllithium; In N,N-dimethyl-formamide;
DOI:10.1021/jo00275a019

Reference yield:

: 122213-31-4
(E)-(R)-3,6-Dimethyl-hept-4-en-1-ol

: 122213-34-7,122292-27-7,122292-28-8,122292-29-9
(E)-(2S,6R)-4-Benzenesulfonyl-2-{(4R,5S,6R)-6-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-6,9-dimethyl-dec-7-en-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triethylamine, methanesulfonyl chloride, 2.) LiBr / 1.) CH₂Cl₂, 0 deg C, 30 min, 2.) acetone, reflux

2: 48 percent / dimethylformamide / Ambient temperature

3: 1.) n-BuLi / 1.) THF, -78 deg C, 45 min, 2.) a) THF, -78 deg C, 50 min, b) 0 deg C, 30 min

With n-butyllithium; methanesulfonyl chloride; triethylamine; lithium bromide; In N,N-dimethyl-formamide;
DOI:10.1021/jo00275a019

Reference yield:

: 122213-30-3
(E)-(R)-3,6-Dimethyl-hept-4-enoic acid methyl ester

: 122213-34-7,122292-27-7,122292-28-8,122292-29-9
(E)-(2S,6R)-4-Benzenesulfonyl-2-{(4R,5S,6R)-6-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-6,9-dimethyl-dec-7-en-3-ol

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄ / diethyl ether / Ambient temperature

2: 1.) triethylamine, methanesulfonyl chloride, 2.) LiBr / 1.) CH₂Cl₂, 0 deg C, 30 min, 2.) acetone, reflux

3: 48 percent / dimethylformamide / Ambient temperature

4: 1.) n-BuLi / 1.) THF, -78 deg C, 45 min, 2.) a) THF, -78 deg C, 50 min, b) 0 deg C, 30 min

With lithium aluminium tetrahydride; n-butyllithium; methanesulfonyl chloride; triethylamine; lithium bromide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jo00275a019