Benzyl-((3E,5E)-1-methyl-hepta-3,5-dienyl)-carbamic acid tert-butyl ester

Base Information

Chemical Name:Benzyl-((3E,5E)-1-methyl-hepta-3,5-dienyl)-carbamic acid tert-butyl ester
CAS No.:98014-61-0
Molecular Formula:C₂₀H₂₉NO₂
Molecular Weight:315.456
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-((3E,5E)-1-methyl-hepta-3,5-dienyl)-carbamic acid tert-butyl ester

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Technology Process of Benzyl-((3E,5E)-1-methyl-hepta-3,5-dienyl)-carbamic acid tert-butyl ester

There total 1 articles about Benzyl-((3E,5E)-1-methyl-hepta-3,5-dienyl)-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98014-60-9
tert-butyl N-benzyl-N-(1-methyl-3-oxopropyl)carbamate

: crotylphosphonium bromide

: 98014-61-0
Benzyl-((3Z,5E)-1-methyl-hepta-3,5-dienyl)-carbamic acid tert-butyl ester

: 98014-62-1
Benzyl-((3E,5E)-1-methyl-hepta-3,5-dienyl)-carbamic acid tert-butyl ester

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, 0 deg C, 30 min., 2.) -78 deg C, 15 min.;
DOI:10.1021/jo00220a026

Reference yield:

: 98014-61-0,98014-62-1
Benzyl-((3E,5E)-1-methyl-hepta-3,5-dienyl)-carbamic acid tert-butyl ester

: 98014-63-2
Benzyl-((3Z,5E)-1-methyl-hepta-3,5-dienyl)-amine

: 98014-64-3
N-benzyl-N-[(4E,6E)-4,6-octadien-2-yl]amine

Guidance literature:: With trimethylsilyl iodide; In dichloromethane; for 20h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo00220a026