Ethyl 2-(1'-phenyl-naphtho<2,1-b>pyrrol-2'-yl)-α-methylcinnamate

Base Information

Chemical Name:Ethyl 2-(1'-phenyl-naphtho<2,1-b>pyrrol-2'-yl)-α-methylcinnamate
CAS No.:146382-52-7
Molecular Formula:C₃₀H₂₅NO₂
Molecular Weight:431.534
Hs Code.:

Synonyms:

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Chemical Property of Ethyl 2-(1'-phenyl-naphtho<2,1-b>pyrrol-2'-yl)-α-methylcinnamate

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Technology Process of Ethyl 2-(1'-phenyl-naphtho<2,1-b>pyrrol-2'-yl)-α-methylcinnamate

There total 6 articles about Ethyl 2-(1'-phenyl-naphtho<2,1-b>pyrrol-2'-yl)-α-methylcinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5392-12-1
2-methoxy-1-naphthaldehyde

: 146382-52-7
Ethyl 2-(1'-phenyl-naphtho<2,1-b>pyrrol-2'-yl)-α-methylcinnamate

Guidance literature:: Multi-step reaction with 5 steps

1: 2.1 g / benzene; diethyl ether / 2 h / 20 °C

2: 0.5 g / HCl / diethyl ether / 24 h / Ambient temperature

3: 425 mg / CH₃MgI / 1) ether, room temp., 1 h, 2) without solvent, 120 deg C, 1 h

4: 145 mg / KOBr / benzene / 2 h / 5 °C

5: 260 mg / NH₂OH*HCl, conc. HCl / tetrahydrofuran / 24 h / Heating

With hydrogenchloride; methyl magnesium iodide; potassium hypobromite; hydroxylamine hydrochloride; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1016/S0040-4020(01)80512-3

Reference yield:

: 146382-40-3
Phenyl-(2-methoxy-1-naphthyl)methanol

: 146382-52-7
Ethyl 2-(1'-phenyl-naphtho<2,1-b>pyrrol-2'-yl)-α-methylcinnamate

Guidance literature:: Multi-step reaction with 4 steps

1: 0.5 g / HCl / diethyl ether / 24 h / Ambient temperature

2: 425 mg / CH₃MgI / 1) ether, room temp., 1 h, 2) without solvent, 120 deg C, 1 h

3: 145 mg / KOBr / benzene / 2 h / 5 °C

4: 260 mg / NH₂OH*HCl, conc. HCl / tetrahydrofuran / 24 h / Heating

With hydrogenchloride; methyl magnesium iodide; potassium hypobromite; hydroxylamine hydrochloride; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1016/S0040-4020(01)80512-3

Reference yield:

: phenylmagnesium bromide

: 146382-52-7
Ethyl 2-(1'-phenyl-naphtho<2,1-b>pyrrol-2'-yl)-α-methylcinnamate

Guidance literature:: Multi-step reaction with 5 steps

1: 2.1 g / benzene; diethyl ether / 2 h / 20 °C

2: 0.5 g / HCl / diethyl ether / 24 h / Ambient temperature

3: 425 mg / CH₃MgI / 1) ether, room temp., 1 h, 2) without solvent, 120 deg C, 1 h

4: 145 mg / KOBr / benzene / 2 h / 5 °C

5: 260 mg / NH₂OH*HCl, conc. HCl / tetrahydrofuran / 24 h / Heating

With hydrogenchloride; methyl magnesium iodide; potassium hypobromite; hydroxylamine hydrochloride; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1016/S0040-4020(01)80512-3