[1,2-diamino(4-chlorobenzyl)ethane](dichloro)platinum(II)

Base Information

Chemical Name:[1,2-diamino(4-chlorobenzyl)ethane](dichloro)platinum(II)
CAS No.:128658-77-5
Molecular Formula:C₉H₁₃Cl₃N₂Pt
Molecular Weight:450.655
Hs Code.:

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Chemical Property of [1,2-diamino(4-chlorobenzyl)ethane](dichloro)platinum(II)

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Technology Process of [1,2-diamino(4-chlorobenzyl)ethane](dichloro)platinum(II)

There total 1 articles about [1,2-diamino(4-chlorobenzyl)ethane](dichloro)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10025-99-7
potassium tetrachloroplatinate(II)

: 104907-20-2
1,2-diamino(4-chlorobenzyl)ethane

: 105856-39-1,128658-77-5,128658-76-4
[1,2-diamino(4-chlorobenzyl)ethane](dichloro)platinum(II)

Guidance literature:: With sodium hydroxide; In water; an aq. soln. of K2PtCl4 was added to a soln. of the ligand in water at pH 6, the mixt. was stirred under successive adjustment of pH to 5-6 with0.1 N NaOH until pH was no longer changed; ppt. was filtered off, washed with water and EtOH and dried;
DOI:10.1016/S0020-1693(02)01490-1

Reference yield: 36.0%

: hematoporphyrin-IX

: 105856-39-1,128658-77-5,128658-76-4
[1,2-diamino(4-chlorobenzyl)ethane](dichloro)platinum(II)

: [1,2-diamino-1-(4-chlorobenzyl)ethane-N,N'][13,17-bis(2-carboxylatoethyl)-3,8-bis(1-hydroxyethyl)-2,7,12,18-tetramethylporphin-O,O']platinum(II)

Guidance literature:: With sodium hydroxide; silver nitrate; In methanol; water; byproducts: AgCl; Sonication; Pt-compd. suspnd. in H2O by stirring and ultrasonication, AgNO3 added, stirred at room temp. for 7 d in the dark, AgCl filtd. off, filtrate was passed through ion exchanger at pH 9 and dropped into MeOH soln. of porphine, stirred at room temp. for 20 h; ppt. was isolated by filtn., washed with water and methanol and dried; elem. anal.;
DOI:10.1016/S0020-1693(02)01490-1