2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium tetraphenylborate

Base Information

• Chemical Name: 2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium tetraphenylborate
• CAS No.: 214531-05-2
• Molecular Formula: C₉H₂₂BN₂O₂*C₂₄H₂₀B
• Molecular Weight: 520.331

Synonyms:

Chemical Property of 2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium tetraphenylborate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium tetraphenylborate

There total 3 articles about 2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium bromide (214530-97-9) + sodium tetraphenyl borate (143-66-8) → 2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium tetraphenylborate (214531-05-2)

Guidance literature:

In water; addn. of NaBPh4 to B-compd.; dissoln. on Me2CO addn., crystn. on concn. (vac.), collection (filtration), washing (water), drying (air-stream); elem. anal.;

DOI:10.1021/ic9713442

Reference yield:

N,N,N'N'-tetramethyl-1,3-propanediamine (110-95-2) → 2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium tetraphenylborate (214531-05-2)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran

2: methanol

3: water

In tetrahydrofuran; methanol; water;

DOI:10.1021/ic9713442

Reference yield:

N,N,N',N'-tetramethylpropanediamine * BH2COOMe (214530-83-3) → 2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium tetraphenylborate (214531-05-2)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol

2: water

In methanol; water;

DOI:10.1021/ic9713442

upstream raw materials:

2-methoxycarbonyl-1,1,3,3-tetramethyl-1,3,2λ(4)-diazaborinanium bromide

sodium tetraphenyl borate

N,N,N'N'-tetramethyl-1,3-propanediamine

N,N,N',N'-tetramethylpropanediamine * BH₂COOMe

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