(4-Nitro-phenyl)-[(6E,8E,15E,17E)-6,8,15,17-tetramethyl-16-(4-nitro-benzoyl)-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecen-7-yl]-methanone

Base Information

• Chemical Name: (4-Nitro-phenyl)-[(6E,8E,15E,17E)-6,8,15,17-tetramethyl-16-(4-nitro-benzoyl)-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecen-7-yl]-methanone
• CAS No.: 118453-52-4
• Molecular Formula: C₃₆H₃₀N₆O₆
• Molecular Weight: 642.671

Synonyms:

Chemical Property of (4-Nitro-phenyl)-[(6E,8E,15E,17E)-6,8,15,17-tetramethyl-16-(4-nitro-benzoyl)-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecen-7-yl]-methanone

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Technology Process of (4-Nitro-phenyl)-[(6E,8E,15E,17E)-6,8,15,17-tetramethyl-16-(4-nitro-benzoyl)-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecen-7-yl]-methanone

There total 1 articles about (4-Nitro-phenyl)-[(6E,8E,15E,17E)-6,8,15,17-tetramethyl-16-(4-nitro-benzoyl)-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecen-7-yl]-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,8-dihydro-5,7,12,14-tetramethyldibenzo<1,4,8,11>tetraazacyclotetradeca-4,6,11,13-tetraene (56276-51-8) + 4-nitro-benzoyl chloride (122-04-3) → (4-Nitro-phenyl)-[(6E,8E,15E,17E)-6,8,15,17-tetramethyl-16-(4-nitro-benzoyl)-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecen-7-yl]-methanone (118453-52-4)

Guidance literature:

With pyridine; In acetonitrile;

DOI:10.1246/cl.1988.1577

Reference yield:

(4-Nitro-phenyl)-[(6E,8E,15E,17E)-6,8,15,17-tetramethyl-16-(4-nitro-benzoyl)-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecen-7-yl]-methanone (118453-52-4) → [(6E,8E,15E,17E)-16-(4-Amino-benzoyl)-6,8,15,17-tetramethyl-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecen-7-yl]-(4-amino-phenyl)-methanone (118453-53-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In 1,4-dioxane;

DOI:10.1246/cl.1988.1577

upstream raw materials:

1,8-dihydro-5,7,12,14-tetramethyldibenzo<1,4,8,11>tetraazacyclotetradeca-4,6,11,13-tetraene

4-nitro-benzoyl chloride

Downstream raw materials:

[(6E,8E,15E,17E)-16-(4-Amino-benzoyl)-6,8,15,17-tetramethyl-5,14-dihydro-5,9,14,18-tetraaza-dibenzo[a,h]cyclotetradecen-7-yl]-(4-amino-phenyl)-methanone

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