(η5-C5Me5)(C6D5)Ir(η1,η3-C3D4)(μ-D)Ir(η5-C5Me5)

Base Information

• Chemical Name: (η5-C5Me5)(C6D5)Ir(η1,η3-C3D4)(μ-D)Ir(η5-C5Me5)
• CAS No.: 116323-58-1
• Molecular Formula: C₂₉H₄₀Ir₂
• Molecular Weight: 782.997
• Mol file: 116323-58-1.mol

Synonyms:

Chemical Property of (η5-C5Me5)(C6D5)Ir(η1,η3-C3D4)(μ-D)Ir(η5-C5Me5)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (η5-C5Me5)(C6D5)Ir(η1,η3-C3D4)(μ-D)Ir(η5-C5Me5)

There total 1 articles about (η5-C5Me5)(C6D5)Ir(η1,η3-C3D4)(μ-D)Ir(η5-C5Me5) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

(η5-C5Me5)(η3-C3H5)(H)Ir (96427-40-6) + benzene-d6 (1076-43-3) → (η5-C5Me5)(C6D5)Ir(η1,η3-C3D4)(μ-D)Ir(η5-C5Me5) (116323-58-1)

Guidance literature:

In a glass bomb (η5-C5Me5)Ir(η3-C3H5)H was reacted with C6D6. The soln. was heated to 50 °C for 17 d. The soln was concd. to 1 ml and heated to 50 °C for 6 d. The residue was dissolved in hexane and cooled to -40 °C.;

DOI:10.1021/ja00233a020

upstream raw materials:

(η5-C5Me5)(η3-C3H5)(H)Ir

benzene-d6