3-[(4-amino-6-{7-chloro-3-oxatricyclo[7.3.1.0^5,13]trideca-1⁽¹³⁾,5,7,9,11-pentaen-8-yl}-1,3,5-triazin-2-yl)sulfanyl]-2,2-dimethylpropanoic acid

Base Information

• Chemical Name: 3-[(4-amino-6-{7-chloro-3-oxatricyclo[7.3.1.0^5,13]trideca-1⁽¹³⁾,5,7,9,11-pentaen-8-yl}-1,3,5-triazin-2-yl)sulfanyl]-2,2-dimethylpropanoic acid
• CAS No.: 1547298-49-6
• Molecular Formula: C₂₀H₁₉ClN₄O₃S
• Molecular Weight: 430.915

Synonyms:

Chemical Property of 3-[(4-amino-6-{7-chloro-3-oxatricyclo[7.3.1.0^5,13]trideca-1⁽¹³⁾,5,7,9,11-pentaen-8-yl}-1,3,5-triazin-2-yl)sulfanyl]-2,2-dimethylpropanoic acid

Chemical Property:

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Technology Process of 3-[(4-amino-6-{7-chloro-3-oxatricyclo[7.3.1.0^5,13]trideca-1⁽¹³⁾,5,7,9,11-pentaen-8-yl}-1,3,5-triazin-2-yl)sulfanyl]-2,2-dimethylpropanoic acid

There total 1 articles about 3-[(4-amino-6-{7-chloro-3-oxatricyclo[7.3.1.0^5,13]trideca-1⁽¹³⁾,5,7,9,11-pentaen-8-yl}-1,3,5-triazin-2-yl)sulfanyl]-2,2-dimethylpropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-2,2-dimethylpropionic acid (2843-17-6) + 4-amino-6-{7-chloro-3-oxatricyclo[7.3.1.05,13]trideca-1(13),5,7,9,11-pentaen-8-yl}-1,3,5-triazine-2-thiol (959762-95-9) → 2,2-dimethyl-3-mercaptopropanoic acid (35040-68-7) + 3-[(4-amino-6-{7-chloro-3-oxatricyclo[7.3.1.05,13]trideca-1(13),5,7,9,11-pentaen-8-yl}-1,3,5-triazin-2-yl)sulfanyl]-2,2-dimethylpropanoic acid (1547298-49-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 80 ℃; for 1h;

DOI:10.1016/j.bmc.2013.11.036

upstream raw materials:

3-bromo-2,2-dimethylpropionic acid

4-amino-6-{7-chloro-3-oxatricyclo[7.3.1.0^5,13]trideca-1⁽¹³⁾,5,7,9,11-pentaen-8-yl}-1,3,5-triazine-2-thiol

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