bis(4-methylphenyl)(9-anthryl)bismuthane

Base Information

Chemical Name:bis(4-methylphenyl)(9-anthryl)bismuthane
CAS No.:192822-79-0
Molecular Formula:C₂₈H₂₃Bi
Molecular Weight:568.471
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(4-methylphenyl)(9-anthryl)bismuthane

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Technology Process of bis(4-methylphenyl)(9-anthryl)bismuthane

There total 1 articles about bis(4-methylphenyl)(9-anthryl)bismuthane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1564-64-3
9-Bromoanthracene

: 7787-58-8
bismuth(III) bromide

: 5142-75-6
tri(p-tolyl)bismuth

: 192822-79-0
bis(4-methylphenyl)(9-anthryl)bismuthane

Guidance literature:: With n-butyllithium; In diethyl ether; Ar-atmosphere; stirring (room temp., 2 h), Bi-compd. soln. addn. (-78°C, stirring), stirring (room temp., 1 h); recrystn. (MeOH); elem. anal.;
DOI:10.1021/om9701377

Reference yield: 88.0%

: 7791-25-5
sulfuryl dichloride

: 192822-79-0
bis(4-methylphenyl)(9-anthryl)bismuthane

: bis(4-methylphenyl)(9-anthryl)bismuth dichloride

Guidance literature:: In dichloromethane; Ar-atmosphere; -78°C to room temp.; evapn. (reduced pressure), recrystn. (CH2Cl2 / hexane); elem. anal.;
DOI:10.1021/om9701377

Reference yield:

: 13709-36-9
xenon difluoride

: 192822-79-0
bis(4-methylphenyl)(9-anthryl)bismuthane

: 441016-81-5
(9-anthryl)di(p-tolyl)difluorobismuth

Guidance literature:: In dichloromethane; to CH2Cl2 soln. (9-anthryl)di(p-tolyl)bismuthine was added CH2Cl2 soln. XeF2 at room temp. and stirred for 10 min; react. mixt. was concd. under reduced pressure and recrystd. from benzene-MeOH; elem. anal.;
DOI:10.1021/om020124f