(C₅H₅)W(CO)3SeCOC₆H₅

Base Information

Chemical Name:(C₅H₅)W(CO)3SeCOC₆H₅
CAS No.:272111-96-3
Molecular Formula:C₁₅H₁₀O₄SeW
Molecular Weight:517.052
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)W(CO)3SeCOC<sub>6</sub>H<sub>5</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₅H₅)W(CO)3SeCOC₆H₅

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Technology Process of (C₅H₅)W(CO)3SeCOC₆H₅

There total 1 articles about (C₅H₅)W(CO)3SeCOC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 7782-49-2
selenium

: 14040-11-0
tungsten hexacarbonyl

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 98-88-4
benzoyl chloride

: tricarbonylcyclopentadienyltungsten(II) chloride

: 272111-96-3
(C₅H₅)W(CO)3SeCOC₆H₅

Guidance literature:: With Na; In tetrahydrofuran; toluene; (under N2, Schlenk); Na refluxed in toluene with stirring, cooled to ambient temp., toluene removed, washed with THF, THF and C5H6 added dropwise at room temp., W(CO)6 added, refluxed, Se added, stirred for 1 h, ligand added, stirred overnight; filtered, solvent removed under vac., ppt. redissolved in CH2Cl2, introduced to silica gel column with hexane, eluted with hexane and CH2Cl2, collected, recrystd. from CH2Cl2/hexane; elem. anal.;
DOI:10.1016/j.ica.2006.06.019