Technology Process of C23H16F3NO3
There total 7 articles about C23H16F3NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
ethanol; water;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/jm201179h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
1.2: 0.5 h / Inert atmosphere
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere
3.1: potassium hydroxide / ethanol; water / 20 °C / Inert atmosphere
With
potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm201179h
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: niobium pentachloride / dichloromethane / 48 h / 20 °C / Inert atmosphere
2.1: acetic acid / ethanol / Inert atmosphere; Reflux
3.1: diphenyl ether-biphenyl eutectic / 0.5 h / 240 °C / Inert atmosphere
4.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
4.2: 0.5 h / Inert atmosphere
5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere
6.1: potassium hydroxide / ethanol; water / 20 °C / Inert atmosphere
With
diphenyl ether-biphenyl eutectic; potassium tert-butylate; niobium pentachloride; acetic acid; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm201179h