α-Chloro-4-bromophenacyl methyl sulfide

Base Information

Chemical Name:α-Chloro-4-bromophenacyl methyl sulfide
CAS No.:1007895-40-0
Molecular Formula:C₉H₈BrClOS
Molecular Weight:279.585
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-Chloro-4-bromophenacyl methyl sulfide

Chemical Property:

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Technology Process of α-Chloro-4-bromophenacyl methyl sulfide

There total 1 articles about α-Chloro-4-bromophenacyl methyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23343-31-9
4-bromo-α-(methylthio)acetophenone

: 1007895-40-0
α-Chloro-4-bromophenacyl methyl sulfide

Guidance literature:: With N-chloro-succinimide; In tetrachloromethane; for 2h; ice-cooling;
DOI:10.1039/b102806p

Reference yield:

: 1007895-40-0
α-Chloro-4-bromophenacyl methyl sulfide

: 128080-99-9
2-[1-(4-Bromobenzoyl)ethyl]-3,4-dimethylthiophene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 448 mg / ZnCl₂ / CH₂Cl₂ / 0.67 h

2.1: 27 percent / Zn; AcOH / 1 h / 100 °C

3.1: LDA / hexane; tetrahydrofuran / 0.83 h / -70 °C

3.2: 48 percent / hexane; tetrahydrofuran / -70 - 0 °C

With acetic acid; zinc(II) chloride; zinc; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; 1.1: Friedel-Crafts reaction;
DOI:10.1039/b102806p

Reference yield:

: 1007895-40-0
α-Chloro-4-bromophenacyl methyl sulfide

: 393085-12-6
2-(4-Bromophenacyl)-3,4-dimethylthiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 448 mg / ZnCl₂ / CH₂Cl₂ / 0.67 h

2: 27 percent / Zn; AcOH / 1 h / 100 °C

With acetic acid; zinc(II) chloride; zinc; In dichloromethane; 1: Friedel-Crafts reaction;
DOI:10.1039/b102806p