[Ir(2,6-bis(N-phenyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2

Base Information

Chemical Name:[Ir(2,6-bis(N-phenyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2
CAS No.:915129-65-6
Molecular Formula:C₆₄H₄₂Cl₄Ir₂N₈
Molecular Weight:1449.34
Hs Code.:

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Chemical Property of [Ir(2,6-bis(N-phenyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2

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Technology Process of [Ir(2,6-bis(N-phenyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2

There total 1 articles about [Ir(2,6-bis(N-phenyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 39823-31-9
1,3-bis(N-phenyl-benzimidazol-2-yl)benzene

: iridium(III) trichloride tetrahydrate

: 915129-65-6
[Ir(2,6-bis(N-phenyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2

Guidance literature:: In methanol; mixt. of Ir compd. and bis(benzimidazolyl)benzene in MeOH refluxed for 5h; cooled to room temp., ppt. sepd., washed with MeOH and ether;
DOI:10.1021/ic060796o

Reference yield: 24.0%

: 1008-89-5
2-phenylpyridine

: 915129-65-6
[Ir(2,6-bis(N-phenyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2

: 7732-18-5
water

: [Ir(2,6-bis(N-phenyl-benzimidazol-2-yl)phenyl-κC1)(2-phenylpyridine(-1H))Cl]*H2O

Guidance literature:: In glycerol; other Radiation; mixt. of Ir complex and pyridine deriv. in glycerol irradiated by microwaves; cooled to room temp., H2O added, ppt. filtered, washed with hexane and ether, chromd. (silica, CH2Cl2/MeOH), recrystd. from CH2Cl2/C6H6/hexane; elem. anal.;
DOI:10.1021/ic060796o