1, 3-bis(1-phenylbenzimidazol-2-yl)benzene

Base Information

• Chemical Name: 1, 3-bis(1-phenylbenzimidazol-2-yl)benzene
• CAS No.: 39823-31-9
• Molecular Formula: C₃₂H₂₂N₄
• Molecular Weight: 462.553
• Mol file: 39823-31-9.mol

Synonyms:1, 3-bis(1-phenylbenzimidazol-2-yl)benzene;1,3-Bis(1-phenyl-1H-benzo[d]iMidazol-2-yl)benzene

Chemical Property of 1, 3-bis(1-phenylbenzimidazol-2-yl)benzene

Chemical Property:

• PSA: 35.64000
• LogP: 7.69840
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

1,3-Bis(1-phenyl-1H-benzo[d]imidazol-2-yl)benzene 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1, 3-bis(1-phenylbenzimidazol-2-yl)benzene

There total 4 articles about 1, 3-bis(1-phenylbenzimidazol-2-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C32H26N4O2 → 1,3-bis(N-phenyl-benzimidazol-2-yl)benzene (39823-31-9)

Guidance literature:

at 290 - 310 ℃; for 2h; Inert atmosphere;

DOI:10.1021/om4007054

Reference yield:

benzene-1,3-dicarbonyl dichloride (99-63-8) → 1,3-bis(N-phenyl-benzimidazol-2-yl)benzene (39823-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1-methyl-pyrrolidin-2-one / 4 h / 20 - 50 °C / Inert atmosphere

2: 2 h / 290 - 310 °C / Inert atmosphere

In 1-methyl-pyrrolidin-2-one;

DOI:10.1021/om4007054

Reference yield:

N-phenyl-1,2-benzenediamine (534-85-0) → 1,3-bis(N-phenyl-benzimidazol-2-yl)benzene (39823-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1-methyl-pyrrolidin-2-one / 4 h / 20 - 50 °C / Inert atmosphere

2: 2 h / 290 - 310 °C / Inert atmosphere

In 1-methyl-pyrrolidin-2-one;

DOI:10.1021/om4007054

upstream raw materials:

benzene-1,3-dicarbonyl dichloride

N-phenyl-1,2-benzenediamine

Downstream raw materials:

[Ir(2,6-bis(N-phenyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2

C₃₂H₂₁IN₄Pt

C₃₃H₂₅N₄OPt⁽¹⁺⁾*CF₃O₃S^(1-)

C₃₂H₂₁ClN₄Pt

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