diag-(η(5)-C5H5)Re(CO)[P(OPh)3]Br2

Base Information

Chemical Name:diag-(η(5)-C5H5)Re(CO)[P(OPh)3]Br2
CAS No.:57139-11-4
Molecular Formula:C₂₄H₂₀Br₂O₄PRe
Molecular Weight:749.409
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Chemical Property of diag-(η(5)-C5H5)Re(CO)[P(OPh)3]Br2

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Technology Process of diag-(η(5)-C5H5)Re(CO)[P(OPh)3]Br2

There total 1 articles about diag-(η(5)-C5H5)Re(CO)[P(OPh)3]Br2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 57139-11-4,57194-45-3
diag-(η(5)-C5H5)Re(CO)[P(OPh)3]Br2

: 57194-45-3,57139-11-4
lat-(η(5)-C5H5)Re(CO)[P(OPh)3]Br2

Guidance literature:: With silica gel; In solid; Irradiation (UV/VIS); Re-compd. dissolved in CH2Cl2 in Pyrex cylinder, silica gel addn., evapn. (vac.), sealed under N2-atmosphere, irradiation (200 W, room temp., 48h, λ > 370 nm); extn. (CH2Cl2), ext. chromy. (SiO2, hexane/CH2Cl2), isolation; identity checked by NMR and IR spectroscopies;
DOI:10.1021/om960726x

Reference yield: 100.0%

: 57139-11-4,57194-45-3
diag-(η(5)-C5H5)Re(CO)[P(OPh)3]Br2

: 57194-45-3,57139-11-4
lat-(η(5)-C5H5)Re(CO)[P(OPh)3]Br2

Guidance literature:: With silica gel; In solid; Irradiation (UV/VIS); Re-compd. dissolved in CH2Cl2 in Pyrex cylinder, silica gel addn., evapn. (vac.), sealed under N2-atmosphere, irradiation (200 W, room temp., 48h, λ > 370 nm); extn. (CH2Cl2), ext. chromy. (SiO2, hexane/CH2Cl2), isolation; identity checked by NMR and IR spectroscopies;
DOI:10.1021/om960726x