cyclohexyl aminepentacarbonylmolybdenum⁽⁰⁾

Base Information

• Chemical Name: cyclohexyl aminepentacarbonylmolybdenum⁽⁰⁾
• CAS No.: 21199-57-5
• Molecular Formula: C₁₁H₁₃MoNO₅
• Molecular Weight: 335.168
• Mol file: 21199-57-5.mol

Synonyms:

Chemical Property of cyclohexyl aminepentacarbonylmolybdenum⁽⁰⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclohexyl aminepentacarbonylmolybdenum⁽⁰⁾

There total 1 articles about cyclohexyl aminepentacarbonylmolybdenum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexylamine (108-91-8,157973-60-9) + molybdenum hexacarbonyl (13939-06-5,199620-15-0) → cyclohexyl aminepentacarbonylmolybdenum(0) (21199-57-5)

Guidance literature:

In decalin; byproducts: CO; N2-atmosphere; excess of amine, 112.00°C; not isolated, reaction followed by IR spectroscopy; Kinetics;

DOI:10.1016/S0020-1693(00)94117-3

Reference yield: 45.4%

cyclohexyl aminepentacarbonylmolybdenum(0) (21199-57-5) → diiodo(cyclohexylamine)molybdenum tetracarbonyl (59993-25-8)

Guidance literature:

With iodine; In hexane; N2-atmosphere; dropwise addn. of 1 equiv. of iodine soln. to Mo-complex soln. (room temp.); elem. anal.;

DOI:10.1016/S0020-1693(00)95609-3

Reference yield: 40.2%

cyclohexyl aminepentacarbonylmolybdenum(0) (21199-57-5) → dibromo(cyclohexylamine)molybdenum tetracarbonyl (59993-26-9)

Guidance literature:

With bromine; In hexane; N2-atmosphere; dropwise addn. of 1 equiv. of bromine soln. to Mo-complexsoln. (room temp.); elem. anal.;

DOI:10.1016/S0020-1693(00)95609-3

upstream raw materials:

cyclohexylamine

molybdenum hexacarbonyl

Downstream raw materials:

bis(maleic anhydride)cyclohexyl aminetricarbonylmolybdenum⁽⁰⁾

dibromo(cyclohexylamine)molybdenum tetracarbonyl

diiodo(cyclohexylamine)molybdenum tetracarbonyl