[Pd(κ2-P,N-7-phospha-3,7-dimethyl-1,3,5-triazobicyclo[3.3.1]nonane)(Me)(acetonitrile)][tetrakis(3,5-difluoromethyl)phenylbo

Base Information

• Chemical Name: [Pd(κ2-P,N-7-phospha-3,7-dimethyl-1,3,5-triazobicyclo[3.3.1]nonane)(Me)(acetonitrile)][tetrakis(3,5-difluoromethyl)phenylbo
• CAS No.: 1054622-61-5
• Molecular Formula: C₁₀H₂₂N₄PPd*C₃₂H₁₂BF₂₄
• Molecular Weight: 1198.93
• Mol file: 1054622-61-5.mol

Synonyms:

Chemical Property of [Pd(κ2-P,N-7-phospha-3,7-dimethyl-1,3,5-triazobicyclo[3.3.1]nonane)(Me)(acetonitrile)][tetrakis(3,5-difluoromethyl)phenylbo

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Pd(κ2-P,N-7-phospha-3,7-dimethyl-1,3,5-triazobicyclo[3.3.1]nonane)(Me)(acetonitrile)][tetrakis(3,5-difluoromethyl)phenylbo

There total 1 articles about [Pd(κ2-P,N-7-phospha-3,7-dimethyl-1,3,5-triazobicyclo[3.3.1]nonane)(Me)(acetonitrile)][tetrakis(3,5-difluoromethyl)phenylbo which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

[Pd(κ2-P,N-7-phospha-3,7-dimethyl-1,3,5-triazobicyclo[3.3.1]nonane)(Me)Cl] (1054622-59-1) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) + acetonitrile (75-05-8,26809-02-9) → [Pd(κ2-P,N-7-phospha-3,7-dimethyl-1,3,5-triazobicyclo[3.3.1]nonane)(Me)(acetonitrile)][tetrakis(3,5-difluoromethyl)phenylbo (1054622-61-5)

Guidance literature:

In dichloromethane; acetonitrile; N2, CH2Cl2/CH3CN (25/1) soln. of Na compd. (0.159 mmol) added to degassed soln. of Pd compd. (0.152 mmol) with stirring, stirred for 1.5 h; filtered (celite), concd., pptd. (Et2O), filtered off, washed (Et2O), dried in N2 flow, elem. anal.;

DOI:10.1016/j.ica.2008.01.051

upstream raw materials:

[Pd(κ2-P,N-7-phospha-3,7-dimethyl-1,3,5-triazobicyclo[3.3.1]nonane)(Me)Cl]

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

acetonitrile