2-acetlyl-η,η(5)-fulvalenedimanganesehexacarbonyl

Base Information

• Chemical Name: 2-acetlyl-η,η(5)-fulvalenedimanganesehexacarbonyl
• CAS No.: 175405-40-0
• Molecular Formula: C₁₈H₁₀Mn₂O₇
• Molecular Weight: 448.149

Synonyms:

Chemical Property of 2-acetlyl-η,η(5)-fulvalenedimanganesehexacarbonyl

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Technology Process of 2-acetlyl-η,η(5)-fulvalenedimanganesehexacarbonyl

There total 1 articles about 2-acetlyl-η,η(5)-fulvalenedimanganesehexacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

η,η(5)-fulvalenedimanganesehexacarbonyl + benzoyl chloride (98-88-4) → 2-acetlyl-η,η(5)-fulvalenedimanganesehexacarbonyl (175405-40-0) + 3-benzoyl-η,η(5)-fulvalenedimanganesehexacarbonyl (175405-41-1)

Guidance literature:

With hydrogenchloride; aluminium trichloride; In dichloromethane; Ar atmosphere; soln. of Mn-compd. dropwise addn. to soln. of Al-compd. and acylchloride, boiling, cooling, decomposition with diluted HCl soln.; solvent elimination from organic layer, column chromy. (Al2O3/benzene-petroleum ether), re-crystn. (heavy petroleum ether); elem. anal.;

DOI:10.1007/BF00707231

upstream raw materials:

benzoyl chloride

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