2-Fluoro-4-(trifluoroMethoxy)benzoyl chloride, 97%

Base Information

• Chemical Name: 2-Fluoro-4-(trifluoroMethoxy)benzoyl chloride, 97%
• CAS No.: 166948-50-1
• Molecular Formula: C₈H₃ClF₄O₂
• Molecular Weight: 242.557
• Hs Code.: 2916399090
• Mol file: 166948-50-1.mol

Synonyms:

Chemical Property of 2-Fluoro-4-(trifluoroMethoxy)benzoyl chloride, 97%

Chemical Property:

• Boiling Point: 203.7±35.0 °C(Predicted)
• Density: 1.511±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

2-Fluoro-4-(trifluoromethoxy)benzoyl chloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Fluoro-4-(trifluoroMethoxy)benzoyl chloride, 97%

There total 1 articles about 2-Fluoro-4-(trifluoroMethoxy)benzoyl chloride, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

2-fluoro-4-(trifluoromethoxy)benzoic acid → 2-fluoro-4-(trifluoromethoxy)benzoyl chloride (166948-50-1)

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

Reference yield: 35.0%

2-fluoro-4-(trifluoromethoxy)benzoyl chloride (166948-50-1) + m-aminobenzenesulfonamide (98-18-0) → 2-fluoro-N-(3-sulfamoylphenyl)-4-(trifluoromethoxy)benzamide

Guidance literature:

With potassium carbonate; In dichloromethane; tert-butyl methyl ether; water; at 0 - 20 ℃; for 0.5h;

Reference yield:

2-fluoro-4-(trifluoromethoxy)benzoyl chloride (166948-50-1) → 2-(4-fluoro-2-methoxyphenoxy)-N-(3-sulfamoylphenyl)-4-(trifluoromethoxy)benzamide

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / dichloromethane; water; tert-butyl methyl ether / 0.5 h / 0 - 20 °C

2: caesium carbonate / 1-methyl-pyrrolidin-2-one / 100 °C

With potassium carbonate; caesium carbonate; In 1-methyl-pyrrolidin-2-one; dichloromethane; tert-butyl methyl ether; water;

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