(tris(diphenylphosphanyl)methane)Au₃Cl₃

Base Information

Chemical Name:(tris(diphenylphosphanyl)methane)Au₃Cl₃
CAS No.:193622-46-7
Molecular Formula:C₃₇H₃₁Au₃Cl₃P₃
Molecular Weight:1265.83
Hs Code.:

(tris(diphenylphosphanyl)methane)Au<sub>3</sub>Cl<sub>3</sub>

Synonyms:

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Chemical Property of (tris(diphenylphosphanyl)methane)Au₃Cl₃

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Technology Process of (tris(diphenylphosphanyl)methane)Au₃Cl₃

There total 2 articles about (tris(diphenylphosphanyl)methane)Au₃Cl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 29892-37-3
chloro(dimethylsulfide) gold(I)

: 28926-65-0
Tris(diphenylphosphino)methan

: 137845-40-0,193622-46-7
[HC(PPh₂)₃Au₃Cl₃]

Guidance literature:: In dichloromethane; N2 atmosphere; addn. of soln. of org. compd. in CH2Cl2 to soln. of Au-compd. (room temp.), stirring (1 h); concn. (vac.), pptn. by addn. of pentane, filtration, washing (pentane), drying (vac.), recrystn. (CH2Cl2/Et2O); elem. anal.;

Reference yield:

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 28926-65-0
Tris(diphenylphosphino)methan

: 193622-46-7,137845-40-0
(tris(diphenylphosphanyl)methane)Au₃Cl₃

Guidance literature:: In not given; (N2);
DOI:10.1021/ic800266m

Reference yield: 96.0%

: tetrakis(acetonitrile)copper(I)tetrafluoroborate

: 193622-46-7,137845-40-0
(tris(diphenylphosphanyl)methane)Au₃Cl₃

: 3034-86-4
4-ethynylbenzoic acid methyl ester

: 1363267-86-0
[(tris(diphenylphosphino)methane)(AuC₂C₆H₄COOCH₃)3Cu]BF₄

Guidance literature:: With triethylamine; In dichloromethane; dropwise addn. of triethylamine to a mixt. of alkyne, Au and Cu complexes in CH2Cl2 under stirring, stirring for 2 h in the dark; concn. in vac., diln. with hexane, filtration, washing ppt. with hexane,ether, drying in vac.; elem. anal.;
DOI:10.1039/c2dt11710j