morpholine amide 3-diphenylphosphinopropionic acid

Base Information

Chemical Name:morpholine amide 3-diphenylphosphinopropionic acid
CAS No.:130648-85-0
Molecular Formula:C₁₉H₂₂NO₂P
Molecular Weight:327.363
Hs Code.:

Synonyms:

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Chemical Property of morpholine amide 3-diphenylphosphinopropionic acid

Chemical Property:

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Technology Process of morpholine amide 3-diphenylphosphinopropionic acid

There total 2 articles about morpholine amide 3-diphenylphosphinopropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 829-85-6
diphenylphosphane

: 130648-85-0
morpholine amide 3-diphenylphosphinopropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / tetraethylammonium hydroxide / acetonitrile / 1 h / Ambient temperature

2: 1.) Me₃Al / 1.) benzene, from -10 deg C to RT, 75 min, 2.) reflux, 20 h

With trimethylaluminum; tetraethylammonium hydroxide; In acetonitrile;
DOI:10.1016/0022-328X(90)87207-T

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 76734-29-7
(3-propionic acid methyl ester)diphenylphosphine

: 130648-85-0
morpholine amide 3-diphenylphosphinopropionic acid

Guidance literature:: With trimethylaluminum; Multistep reaction; 1.) benzene, from -10 deg C to RT, 75 min, 2.) reflux, 20 h;
DOI:10.1016/0022-328X(90)87207-T

Reference yield:

: sodium tetrachloropalladate(II)

: 130648-85-0
morpholine amide 3-diphenylphosphinopropionic acid

: PdCl₂(Ph₂Pmorph)2*0.25CH₂Cl₂

Guidance literature:: In ethanol; stirred at ambient conditions for 4 h; precipitate filtered, dried, crystallized from CH2Cl2/ethanol/heptane, elem. anal., ratio of cis/trans:10/90;
DOI:10.1016/0022-328X(90)87207-T