C₂₉H₃₆N₂O₅S

Base Information

Chemical Name:C₂₉H₃₆N₂O₅S
CAS No.:1360744-13-3
Molecular Formula:C₂₉H₃₆N₂O₅S
Molecular Weight:524.681
Hs Code.:

C<sub>29</sub>H<sub>36</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₉H₃₆N₂O₅S

Chemical Property:

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Technology Process of C₂₉H₃₆N₂O₅S

There total 15 articles about C₂₉H₃₆N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360744-09-7
C₁₂H₁₈O₄

: 1360744-13-3
C₂₉H₃₆N₂O₅S

Guidance literature:: Multi-step reaction with 12 steps

1.1: hydrogen iodide / water; toluene / 0.5 h / 0 - 20 °C

1.2: 2 h / Reflux

2.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

4.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

5.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

5.2: 1 h / 0 - 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

6.2: 3 h / 20 °C

7.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

8.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

9.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

10.1: zinc dibromide / dichloromethane / 2 h / Inert atmosphere; Reflux

11.1: triethylamine / dichloromethane / 10 h

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran

With 1H-imidazole; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen iodide; tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; triethylamine; platinum(II) chloride; zinc dibromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil; 3.1: Sonogashira coupling / 5.1: Hydroboration reaction / 7.1: Barton-McCombie deoxygenation / 9.1: Wittig reaction;
DOI:10.1002/chem.201102101

Reference yield:

: 1360744-10-0
C₇H₉IO₂

: 1360744-13-3
C₂₉H₃₆N₂O₅S

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

3.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

4.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

4.2: 1 h / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

5.2: 3 h / 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

8.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

9.1: zinc dibromide / dichloromethane / 2 h / Inert atmosphere; Reflux

10.1: triethylamine / dichloromethane / 10 h

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran

With 1H-imidazole; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; potassium tert-butylate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; triethylamine; platinum(II) chloride; zinc dibromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil; 2.1: Sonogashira coupling / 4.1: Hydroboration reaction / 6.1: Barton-McCombie deoxygenation / 8.1: Wittig reaction;
DOI:10.1002/chem.201102101

Reference yield:

: 1360744-06-4
C₂₁H₂₆N₂O₆S

: 1360744-13-3
C₂₉H₃₆N₂O₅S

Guidance literature:: Multi-step reaction with 10 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

2.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

3.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

3.2: 1 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

4.2: 3 h / 20 °C

5.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

6.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

7.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

8.1: zinc dibromide / dichloromethane / 2 h / Inert atmosphere; Reflux

9.1: triethylamine / dichloromethane / 10 h

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; potassium tert-butylate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; triethylamine; platinum(II) chloride; zinc dibromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil; 1.1: Sonogashira coupling / 3.1: Hydroboration reaction / 5.1: Barton-McCombie deoxygenation / 7.1: Wittig reaction;
DOI:10.1002/chem.201102101