ButanaMide, 4-aMino-N,N-diethyl-

Base Information

• Chemical Name: ButanaMide, 4-aMino-N,N-diethyl-
• CAS No.: 104970-81-2
• Molecular Formula: C₈H₁₈N₂O
• Molecular Weight: 158.244
• Mol file: 104970-81-2.mol

Synonyms:

Chemical Property of ButanaMide, 4-aMino-N,N-diethyl-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ButanaMide, 4-aMino-N,N-diethyl-

There total 10 articles about ButanaMide, 4-aMino-N,N-diethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-diethyl-2,2-difluoro-4-nitrobutanamide (1361968-69-5) → C8H18N2O (104970-81-2) + 3,3-difluoropyrrolidin-2-one (162970-49-2)

Guidance literature:

With platinum on carbon; In toluene; at 50 ℃; for 24h; under 3345.86 Torr;

DOI:10.1016/j.jfluchem.2011.08.009

Reference yield:

N,N-diethyl-2,2-difluoro-4-nitrobutanamide (1361968-69-5) → C8H18N2O (104970-81-2) + C8H16F2N2O (1361968-70-8) + 3,3-difluoropyrrolidin-2-one (162970-49-2)

Guidance literature:

With platinum on carbon; In methanol; at 60 ℃; for 24h; under 4380.18 Torr;

DOI:10.1016/j.jfluchem.2011.08.009

Reference yield:

C10H16F2N2O5 → C8H18N2O (104970-81-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 20 °C

2: platinum on carbon / toluene / 24 h / 50 °C / 3345.86 Torr

With sodium tetrahydroborate; platinum on carbon; In ethanol; toluene;

DOI:10.1016/j.jfluchem.2011.08.009

upstream raw materials:

N,N-diethyl-2,2-difluoro-4-nitrobutanamide

2-chloro-N,N-diethyl-2,2-difluoroacetamide

3-ethoxy-N,N-diethyl-2,2-difluoro-3-hydroxypropionamide

N,N-diethyl-2,2-difluoro-3-hydroxy-4-nitrobutanamide

Refernces