C₂₁H₃₄INO₃

Base Information

Chemical Name:C₂₁H₃₄INO₃
CAS No.:1265966-34-4
Molecular Formula:C₂₁H₃₄INO₃
Molecular Weight:475.41
Hs Code.:

C<sub>21</sub>H<sub>34</sub>INO<sub>3</sub>

Synonyms:

Suppliers and Price of C₂₁H₃₄INO₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₃₄INO₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of C₂₁H₃₄INO₃

There total 1 articles about C₂₁H₃₄INO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-22-1
n-Dodecylamine

: 1265966-33-3
C₉H₉IO₄

: 1265966-34-4
C₂₁H₃₄INO₃

Guidance literature:: C₉H₉IO₄; With 6-chloro-1-hydroxybenzotriazole; diisopropyl-carbodiimide; In tetrahydrofuran; at 60 ℃; for 0.666667h; Inert atmosphere;

n-Dodecylamine; In tetrahydrofuran; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c2cc35087d

Reference yield:

: 1265966-34-4
C₂₁H₃₄INO₃

: 1416366-84-1
C₆₂H₉₆N₂O₆Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / Sonication

2: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) iodide / 20 °C / Inert atmosphere

3: potassium carbonate / tetrahydrofuran; methanol / 0.25 h

4: N,N,N,N,-tetramethylethylenediamine; copper(l) chloride / acetone / 2 h / 50 °C

With 1H-imidazole; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; potassium carbonate; triethylamine; copper(l) chloride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; 2: |Sonogashira Cross-Coupling / 4: |Hay Coupling;
DOI:10.1039/c2cc35087d

Reference yield:

: 1265966-34-4
C₂₁H₃₄INO₃

: 1402085-25-9
C₅₀H₆₈N₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / Sonication

2: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) iodide / 20 °C / Inert atmosphere

3: potassium carbonate / tetrahydrofuran; methanol / 0.25 h

4: N,N,N,N,-tetramethylethylenediamine; copper(l) chloride / acetone / 2 h / 50 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

With 1H-imidazole; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; copper(l) chloride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; 2: |Sonogashira Cross-Coupling / 4: |Hay Coupling;
DOI:10.1039/c2cc35087d