N-Acetyl-N-(acetyloxy)-alpha-chlorobenzeneacetamide

Base Information

Chemical Name:N-Acetyl-N-(acetyloxy)-alpha-chlorobenzeneacetamide
CAS No.:77130-76-8
Molecular Formula:C₁₂H₁₂ClNO₄
Molecular Weight:269.685
Hs Code.:
DSSTox Substance ID:DTXSID901241280

Synonyms:N-Acetyl-N-(acetyloxy)-alpha-chlorobenzeneacetamide;DTXSID901241280;77130-76-8

Suppliers and Price of N-Acetyl-N-(acetyloxy)-alpha-chlorobenzeneacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N-Acetyl-N-(acetyloxy)-alpha-chlorobenzeneacetamide

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:269.0454856
Heavy Atom Count:18
Complexity:339

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)N(C(=O)C(C1=CC=CC=C1)Cl)OC(=O)C

Technology Process of N-Acetyl-N-(acetyloxy)-alpha-chlorobenzeneacetamide

There total 3 articles about N-Acetyl-N-(acetyloxy)-alpha-chlorobenzeneacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 108-24-7
acetic anhydride

: 77130-74-6
acide N-acetyl chloro-2 phenyl-2 acetohydroxamique

: 77130-76-8
N,O-diacetyk N-(α-chloro phenacetyl) hydroxylamine

Guidance literature:: at 100 ℃; for 1h;
DOI:10.1016/0040-4020(80)80224-9

Reference yield:

: 102-96-5
(2-nitroethenyl)benzene

: 77130-76-8
N,O-diacetyk N-(α-chloro phenacetyl) hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent Spectr_. / FeCl₃ / CH₂Cl₂ / 0 °C

2: 82 percent / 1 h / 100 °C

iron(III) chloride; In dichloromethane;
DOI:10.1016/0040-4020(80)80224-9