1,11-Bis-(di-p-anisyl-phosphinomethyl)-benzophenanthren

Base Information

Chemical Name:1,11-Bis-(di-p-anisyl-phosphinomethyl)-benzophenanthren
CAS No.:65796-60-3
Molecular Formula:C₄₈H₄₂O₄P₂
Molecular Weight:744.807
Hs Code.:

1,11-Bis-(di-p-anisyl-phosphinomethyl)-benzo<c>phenanthren

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,11-Bis-(di-p-anisyl-phosphinomethyl)-benzophenanthren

Chemical Property:

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Technology Process of 1,11-Bis-(di-p-anisyl-phosphinomethyl)-benzophenanthren

There total 3 articles about 1,11-Bis-(di-p-anisyl-phosphinomethyl)-benzophenanthren which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66082-71-1
1,11-Bis-(di-p-anisyl-phosphorylmethyl)-benzophenanthren

: 65796-60-3
1,11-Bis-(di-p-anisyl-phosphinomethyl)-benzophenanthren

Guidance literature:: With tributyl-amine; trichlorosilane; In acetonitrile; Heating;
DOI:10.1002/hlca.19770600835

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 65796-60-3
1,11-Bis-(di-p-anisyl-phosphinomethyl)-benzophenanthren

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Mg, Et₂O, (ii) HPO(OEt)2, (iii) aq. HCl

2: (i) nBuLi, hexane, THF, (ii) /BRN= 2535167/

3: HSiCl₃, nBu₃N / acetonitrile / Heating

With tributyl-amine; trichlorosilane; In acetonitrile;
DOI:10.1002/hlca.19770600835

Reference yield:

: 15754-51-5
bis(4-methoxyphenyl)phosphine oxide

: 65796-60-3
1,11-Bis-(di-p-anisyl-phosphinomethyl)-benzophenanthren

Guidance literature:: Multi-step reaction with 2 steps

1: (i) nBuLi, hexane, THF, (ii) /BRN= 2535167/

2: HSiCl₃, nBu₃N / acetonitrile / Heating

With tributyl-amine; trichlorosilane; In acetonitrile;
DOI:10.1002/hlca.19770600835