trans-(1S(R),2S(R))-2-hydroxycyclohexyl nitrate

Base Information

• Chemical Name: trans-(1S(R),2S(R))-2-hydroxycyclohexyl nitrate
• CAS No.: 32342-26-0
• Molecular Formula: C₆H₁₁NO₄
• Molecular Weight: 161.158

Synonyms:

Chemical Property of trans-(1S(R),2S(R))-2-hydroxycyclohexyl nitrate

Chemical Property:

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Technology Process of trans-(1S(R),2S(R))-2-hydroxycyclohexyl nitrate

There total 6 articles about trans-(1S(R),2S(R))-2-hydroxycyclohexyl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

cyclohexane-1,2-epoxide (286-20-4) → trans-(1S(R),2S(R))-2-hydroxycyclohexyl nitrate (32342-26-0,32342-27-1,75561-13-6)

Guidance literature:

With bismuth(III) nitrate; In acetonitrile; at 20 ℃; for 0.333333h;

DOI:10.1002/hlca.200790002

Reference yield: 85.0%

cyclohexane-1,2-epoxide (286-20-4) → trans-(1S(R),2S(R))-2-hydroxycyclohexyl nitrate (32342-26-0,32342-27-1,75561-13-6) + 2-nitrosooxy-cyclohexanol

Guidance literature:

With sodium nitrate; cerium(IV) triflate; sodium dodecyl-sulfate; at 20 ℃; for 0.5h;

DOI:10.1039/b211697a

Reference yield:

cis-1,2-cyclohexane (1792-81-0) → (+/-)-cis-2-Nitryloxy-cyclohexanol (32342-26-0,32342-27-1,75561-13-6)

Guidance literature:

With nitric acid; In acetic anhydride; at 0 - 20 ℃; for 2.5h;

DOI:10.1021/jo9809130

upstream raw materials:

cis-1,2-cyclohexane

cyclohexane-1,2-epoxide

cyclohexene oxide

trans-1,2-cyclohexandiol

Downstream raw materials:

(+)-trans-1-acetoxy-2-nitroxycyclohexane

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