2-[1-(4-chlorophenyl)propyl]malonic acid

Base Information

Chemical Name:2-[1-(4-chlorophenyl)propyl]malonic acid
CAS No.:82756-60-3
Molecular Formula:C₁₂H₁₃ClO₄
Molecular Weight:256.686
Hs Code.:
Mol file:82756-60-3.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[1-(4-chlorophenyl)propyl]malonic acid

Chemical Property:

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Technology Process of 2-[1-(4-chlorophenyl)propyl]malonic acid

There total 4 articles about 2-[1-(4-chlorophenyl)propyl]malonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102733-43-7
diethyl 2-(1-(4-chlorophenyl)propyl)malonate

: 82756-60-3
1-(4-Chlorphenyl)-propylmalonsaeure

Guidance literature:: With potassium hydroxide; In ethanol; Heating;
DOI:10.1135/cccc19760633

Reference yield:

: 6285-05-8
4'-chloropropiophenone

: 82756-60-3
1-(4-Chlorphenyl)-propylmalonsaeure

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄, aq. NaOH / methanol

2: PBr₃, Py / diethyl ether

3: NaOEt / ethanol

4: aq. KOH / ethanol / Heating

With pyridine; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; sodium ethanolate; phosphorus tribromide; In methanol; diethyl ether; ethanol;
DOI:10.1135/cccc19760633

Reference yield:

: 13856-85-4
1-(4-chlorophenyl)-1-propanol

: 82756-60-3
1-(4-Chlorphenyl)-propylmalonsaeure

Guidance literature:: Multi-step reaction with 3 steps

1: PBr₃, Py / diethyl ether

2: NaOEt / ethanol

3: aq. KOH / ethanol / Heating

With pyridine; potassium hydroxide; sodium ethanolate; phosphorus tribromide; In diethyl ether; ethanol;
DOI:10.1135/cccc19760633