C₂₄H₂₈N₂O₃

Base Information

Chemical Name:C₂₄H₂₈N₂O₃
CAS No.:145387-93-5
Molecular Formula:C₂₄H₂₈N₂O₃
Molecular Weight:392.498
Hs Code.:

C<sub>24</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₄H₂₈N₂O₃

Chemical Property:

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Technology Process of C₂₄H₂₈N₂O₃

There total 20 articles about C₂₄H₂₈N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124981-58-4
1-(2-Methoxy-ethyl)-cyclohexa-2,5-dienecarboxylic acid

: 145387-93-5
C₂₄H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 20 steps

1: 1) (PhO)2P(=O)N₃, Et₃N, pyrrolidine; 2) I₂, H₂O / 2) THF

2: 2,2'-azobisisobutyronitrile / benzene / Ambient temperature

4: 4-(N,N-dimethylamino)pyridine, pyridine

6: BBr₃

7: Swern oxidation

9: 68 percent / H₂, pyridine / BaSO₄

10: 86 percent / Ph₃P, diethyl azodicarboxylate

11: (CH₃)3SiCl, NaI / acetonitrile

12: Et₃N, 4-(N,N-dimethylamino)pyridine / CH₂Cl₂

13: 91 percent / KH, 18-crown-6, tetra-n-butylammonium iodide

14: LiOH

15: VO(acac)2, t-BuOOH / Heating

16: 86 percent / Hunig's base

17: 72 percent / CsF / dimethylformamide / Heating

18: 93 percent / 4-(N,N-dimethylamino)pyridine, Et₃N

19: 65 percent / Me₃SiCl, NaI / acetonitrile

20: 2) basic alumina / 1) Swern oxidation

With pyrrolidine; pyridine; tert.-butylhydroperoxide; dmap; aluminum oxide; lithium hydroxide; chloro-trimethyl-silane; bis(acetylacetonate)oxovanadium; 18-crown-6 ether; 2,2'-azobis(isobutyronitrile); diphenyl phosphoryl azide; water; hydrogen; iodine; boron tribromide; tetra-(n-butyl)ammonium iodide; potassium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; cesium fluoride; sodium iodide; diethylazodicarboxylate; barium sulfate; In dichloromethane; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1016/S0040-4039(00)60944-9

Reference yield:

: 145387-74-2
(1R,5R,8R)-8-Iodo-1-(2-methoxy-ethyl)-6-oxa-bicyclo[3.2.1]oct-2-en-7-one

: 145387-93-5
C₂₄H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 19 steps

1: 2,2'-azobisisobutyronitrile / benzene / Ambient temperature

3: 4-(N,N-dimethylamino)pyridine, pyridine

5: BBr₃

6: Swern oxidation

8: 68 percent / H₂, pyridine / BaSO₄

9: 86 percent / Ph₃P, diethyl azodicarboxylate

10: (CH₃)3SiCl, NaI / acetonitrile

11: Et₃N, 4-(N,N-dimethylamino)pyridine / CH₂Cl₂

12: 91 percent / KH, 18-crown-6, tetra-n-butylammonium iodide

13: LiOH

14: VO(acac)2, t-BuOOH / Heating

15: 86 percent / Hunig's base

16: 72 percent / CsF / dimethylformamide / Heating

17: 93 percent / 4-(N,N-dimethylamino)pyridine, Et₃N

18: 65 percent / Me₃SiCl, NaI / acetonitrile

19: 2) basic alumina / 1) Swern oxidation

With pyridine; tert.-butylhydroperoxide; dmap; aluminum oxide; lithium hydroxide; chloro-trimethyl-silane; bis(acetylacetonate)oxovanadium; 18-crown-6 ether; 2,2'-azobis(isobutyronitrile); hydrogen; boron tribromide; tetra-(n-butyl)ammonium iodide; potassium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; cesium fluoride; sodium iodide; diethylazodicarboxylate; barium sulfate; In dichloromethane; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1016/S0040-4039(00)60944-9

Reference yield:

: (1S,5R,6S)-6-Allyl-5-hydroxy-1-(2-methoxy-ethyl)-cyclohex-2-enecarboxylic acid (4-methoxy-phenyl)-amide

: 145387-93-5
C₂₄H₂₈N₂O₃

Guidance literature:: Multi-step reaction with 17 steps

1: 4-(N,N-dimethylamino)pyridine, pyridine

3: BBr₃

4: Swern oxidation

6: 68 percent / H₂, pyridine / BaSO₄

7: 86 percent / Ph₃P, diethyl azodicarboxylate

8: (CH₃)3SiCl, NaI / acetonitrile

9: Et₃N, 4-(N,N-dimethylamino)pyridine / CH₂Cl₂

10: 91 percent / KH, 18-crown-6, tetra-n-butylammonium iodide

11: LiOH

12: VO(acac)2, t-BuOOH / Heating

13: 86 percent / Hunig's base

14: 72 percent / CsF / dimethylformamide / Heating

15: 93 percent / 4-(N,N-dimethylamino)pyridine, Et₃N

16: 65 percent / Me₃SiCl, NaI / acetonitrile

17: 2) basic alumina / 1) Swern oxidation

With pyridine; tert.-butylhydroperoxide; dmap; aluminum oxide; lithium hydroxide; chloro-trimethyl-silane; bis(acetylacetonate)oxovanadium; 18-crown-6 ether; hydrogen; boron tribromide; tetra-(n-butyl)ammonium iodide; potassium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; cesium fluoride; sodium iodide; diethylazodicarboxylate; barium sulfate; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(00)60944-9