Carbonic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Base Information

• Chemical Name: Carbonic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
• CAS No.: 108311-35-9
• Molecular Formula: C₂₈H₃₅N₅O₆
• Molecular Weight: 537.616

Synonyms:

Chemical Property of Carbonic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbonic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

There total 3 articles about Carbonic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Carbonic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester → Carbonic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (108311-35-9)

Guidance literature:

With benzenesulfonic acid; In methanol; chloroform; Yield given;

DOI:10.1016/S0040-4039(00)85202-8

Reference yield:

(1R,2S,5R)-menthyl chloroformate (14602-86-9,7635-53-2) → Carbonic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (108311-35-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethy-aminopyridine / CH₂Cl₂ / Ambient temperature; overnight

2: 2percent benzenesulfonic acid / methanol; CHCl₃

With dimethy-aminopyridine; benzenesulfonic acid; In methanol; dichloromethane; chloroform;

DOI:10.1016/S0040-4039(00)85202-8

Reference yield:

N6-benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine (64325-78-6) → Carbonic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (108311-35-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethy-aminopyridine / CH₂Cl₂ / Ambient temperature; overnight

2: 2percent benzenesulfonic acid / methanol; CHCl₃

With dimethy-aminopyridine; benzenesulfonic acid; In methanol; dichloromethane; chloroform;

DOI:10.1016/S0040-4039(00)85202-8

upstream raw materials:

(1R,2S,5R)-menthyl chloroformate

N₆-benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine

Downstream raw materials:

C₆₀H₆₈N₇O₁₄P

C₆₀H₆₈N₇O₁₄P

C₆₆H₇₁N₈O₁₄P

C₆₆H₇₁N₈O₁₄P

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