Diisopropyl-phosphoramidous acid (2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester

Base Information

Chemical Name:Diisopropyl-phosphoramidous acid (2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester
CAS No.:338800-86-5
Molecular Formula:C₄₆H₅₃N₄O₆P
Molecular Weight:788.924
Hs Code.:

Diisopropyl-phosphoramidous acid (2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester

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Chemical Property of Diisopropyl-phosphoramidous acid (2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester

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Technology Process of Diisopropyl-phosphoramidous acid (2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester

There total 1 articles about Diisopropyl-phosphoramidous acid (2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102691-36-1
N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

: 338800-85-4
(2R,3S,5R)-5-[2,2']Bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-ol

: 338800-86-5
Diisopropyl-phosphoramidous acid (2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester

Guidance literature:: With 1H-tetrazole; In acetonitrile; for 1.5h;
DOI:10.1039/b009855h

Reference yield:

: 338800-86-5
Diisopropyl-phosphoramidous acid (2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2-cyano-ethyl ester

: 338800-88-7
Acetic acid (2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[{(2R,3S,5R)-5-[2,2']bipyridinyl-5-ylmethyl-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-(2-cyano-ethoxy)-phosphoryloxymethyl]-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / acetonitrile / 3 h

2: I₂; H₂O; pyridine / tetrahydrofuran

With pyridine; 1H-tetrazole; water; iodine; In tetrahydrofuran; acetonitrile;
DOI:10.1039/b009855h