(2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl)-4-aminophenylmethane

Base Information

Chemical Name:(2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl)-4-aminophenylmethane
CAS No.:161909-26-8
Molecular Formula:C₂₁H₂₇NO₉
Molecular Weight:437.447
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl)-4-aminophenylmethane

Chemical Property:

Purity/Quality:

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Technology Process of (2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl)-4-aminophenylmethane

There total 6 articles about (2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl)-4-aminophenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67773-43-7
2,3,4,6-tetra-O-benzyl-α/β-D-glucopyranosyl bromide

: 161909-26-8
(2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl)-4-aminophenylmethane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg / 2.) ether, reflux, 4 h

2: H₂ / 10percent Pd-C / acetic acid / 19 h / 2068.6 Torr

3: pyridine / 16 h

4: 1.) Ac₂O, Cu(NO₃)2, 2.) H₂ / 2.) 10percent Pd-C / 2.) methanol

With pyridine; hydrogen; acetic anhydride; copper(II) nitrate; magnesium; palladium on activated charcoal; In acetic acid;

Reference yield:

: 100-44-7
benzyl chloride

: 161909-26-8
(2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl)-4-aminophenylmethane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg / 2.) ether, reflux, 4 h

2: H₂ / 10percent Pd-C / acetic acid / 19 h / 2068.6 Torr

3: pyridine / 16 h

4: 1.) Ac₂O, Cu(NO₃)2, 2.) H₂ / 2.) 10percent Pd-C / 2.) methanol

With pyridine; hydrogen; acetic anhydride; copper(II) nitrate; magnesium; palladium on activated charcoal; In acetic acid;

Reference yield:

: 54423-54-0
2,3,4,6-Tetra-O-benzyl 1-O-p-nitrobenzoyl D-glucopyranoside

: 161909-26-8
(2,3,4,6-Tetra-O-acetyl-β-D-glucopyranosyl)-4-aminophenylmethane

Guidance literature:: Multi-step reaction with 5 steps

1: HBr / CH₂Cl₂ / 0.17 h

2: 1.) Mg / 2.) ether, reflux, 4 h

3: H₂ / 10percent Pd-C / acetic acid / 19 h / 2068.6 Torr

4: pyridine / 16 h

5: 1.) Ac₂O, Cu(NO₃)2, 2.) H₂ / 2.) 10percent Pd-C / 2.) methanol

With pyridine; hydrogen bromide; hydrogen; acetic anhydride; copper(II) nitrate; magnesium; palladium on activated charcoal; In dichloromethane; acetic acid;