1-{O₆-[3'-O-alloxycarbonyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-4-{O₆-[3'-O-tertbutyldimethylsilyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-butane

Base Information

• Chemical Name: 1-{O₆-[3'-O-alloxycarbonyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-4-{O₆-[3'-O-tertbutyldimethylsilyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-butane
• CAS No.: 1254514-28-7
• Molecular Formula: C₉₂H₉₈N₁₀O₁₈Si
• Molecular Weight: 1659.93

Synonyms:

Chemical Property of 1-{O₆-[3'-O-alloxycarbonyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-4-{O₆-[3'-O-tertbutyldimethylsilyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-butane

Chemical Property:

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Useful:

Technology Process of 1-{O₆-[3'-O-alloxycarbonyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-4-{O₆-[3'-O-tertbutyldimethylsilyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-butane

There total 1 articles about 1-{O₆-[3'-O-alloxycarbonyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-4-{O₆-[3'-O-tertbutyldimethylsilyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-2'-deoxyguanidyl]}-butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.1%

3’-O-(tertbutyldimethylsilyl)-5’-O-(4,4’-dimethoxytrityl)-N2-phenoxyacetyl-2’-deoxyguanosine (642462-83-7) + 3'-O-alloxycarbonyl-5'-O-dimethoxytrityl-N2-phenoxyacetyl-O6-(4-hydroxybutyl)-2'-deoxyguanosine (1134987-36-2) → 1-{O6-[3'-O-alloxycarbonyl-5'-O-dimethoxytrityl-N2-phenoxyacetyl-2'-deoxyguanidyl]}-4-{O6-[3'-O-tertbutyldimethylsilyl-5'-O-dimethoxytrityl-N2-phenoxyacetyl-2'-deoxyguanidyl]}-butane (1254514-28-7)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In 1,4-dioxane; for 14h;

DOI:10.1039/c0ob00093k

upstream raw materials:

3’-O-(tertbutyldimethylsilyl)-5’-O-(4,4’-dimethoxytrityl)-N2-phenoxyacetyl-2’-deoxyguanosine

3'-O-alloxycarbonyl-5'-O-dimethoxytrityl-N₂-phenoxyacetyl-O₆-(4-hydroxybutyl)-2'-deoxyguanosine

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