PtS(P(C₆H₅)3)2

Base Information

Chemical Name:PtS(P(C₆H₅)3)2
CAS No.:70341-28-5
Molecular Formula:C₃₆H₃₀P₂PtS
Molecular Weight:751.728
Hs Code.:

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Chemical Property of PtS(P(C₆H₅)3)2

Chemical Property:

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Technology Process of PtS(P(C₆H₅)3)2

There total 5 articles about PtS(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 10544-50-0
sulfur

: 14221-02-4
tetrakis(triphenylphosphine)platinum⁽⁰⁾

: 70341-28-5
PtS(P(C₆H₅)3)2

Guidance literature:: In benzene; byproducts: triphenylphosphine sulfide; Pt complex adding to a frozen, degassed sulfur suspn. in benzene in a molar ratio 1:1 under N2, stirring for 5 h; the solid washing with benzene and hexane and air drying;

Reference yield: 43.0%

: 12120-15-9
Pt(PPh₃)2(C₂H₄)

: 29449-10-3
PtS₄(P(C₆H₅)3)2

: 70341-28-5
PtS(P(C₆H₅)3)2

Guidance literature:: In benzene; 3 equiv of ethylene Pt complex adding to 1 equiv of polysulfide Pt complex in degassed benzene under N2, stirring for 60 h, orange solid filtering off; identified by elem. anal.;

Reference yield: 40.0%

: 10544-50-0
sulfur

: 14221-02-4
tetrakis(triphenylphosphine)platinum⁽⁰⁾

: PtS₄(P(C₆H₅)3)2*0.25CH₂Cl₂

: 70341-28-5
PtS(P(C₆H₅)3)2

Guidance literature:: With CH₂Cl₂; In benzene; byproducts: triphenylphosphine sulfide; Pt complex adding to a frozen, degassed sulfur suspn. in benzene in a molar ratio 1:4 under N2, stirring for 5 h; the solid washing with benzene and hexane and air drying; dissolving in CH2Cl2, filtering, treating with EtOH, concg., crystals sepg.; identified by elem. anal. and NMR spectrum;