[2-(1H-pyrazolyl-κN2)-6-((diphenylphosphino)amine-κP)phenyl-κCl]palladium(II) chloride

Base Information

Chemical Name:[2-(1H-pyrazolyl-κN2)-6-((diphenylphosphino)amine-κP)phenyl-κCl]palladium(II) chloride
CAS No.:1033630-77-1
Molecular Formula:C₂₁H₁₇ClN₃PPd
Molecular Weight:484.233
Hs Code.:

Synonyms:

Suppliers and Price of [2-(1H-pyrazolyl-κN2)-6-((diphenylphosphino)amine-κP)phenyl-κCl]palladium(II) chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [2-(1H-pyrazolyl-κN2)-6-((diphenylphosphino)amine-κP)phenyl-κCl]palladium(II) chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [2-(1H-pyrazolyl-κN2)-6-((diphenylphosphino)amine-κP)phenyl-κCl]palladium(II) chloride

There total 1 articles about [2-(1H-pyrazolyl-κN2)-6-((diphenylphosphino)amine-κP)phenyl-κCl]palladium(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 184097-88-9
3-(1H-pyrazol-1-yl)aniline

: 1033630-77-1
[2-(1H-pyrazolyl-κN2)-6-((diphenylphosphino)amine-κP)phenyl-κCl]palladium(II) chloride

Guidance literature:: With triethylamine; In hexane; toluene; under Ar atm. soln. ClPPh2 in toluene was added dropwise to soln. amine and Et3N in toluene-hexane at room temp. and stirred for 10 h, added to suspn. Pd complex in toluene and heated to reflux for 4 h; soln. was filtered and concd. in vacuo, residue was dissolved in acetoneand cooled to -20°C; elem. anal.;
DOI:10.1021/om800175a