C₂HF₃O₂*C₁₇H₂₀N₂O

Base Information

Chemical Name:C₂HF₃O₂*C₁₇H₂₀N₂O
CAS No.:1368806-99-8
Molecular Formula:C₂HF₃O₂*C₁₇H₂₀N₂O
Molecular Weight:382.383
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>17</sub>H<sub>20</sub>N<sub>2</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂HF₃O₂*C₁₇H₂₀N₂O

Chemical Property:

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Technology Process of C₂HF₃O₂*C₁₇H₂₀N₂O

There total 5 articles about C₂HF₃O₂*C₁₇H₂₀N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-phenylbut-3-yn-2-one O-methyl oxime

: 1368806-99-8
C₂HF₃O₂*C₁₇H₂₀N₂O

Guidance literature:: Multi-step reaction with 3 steps

1: Iodine monochloride / dichloromethane / 20 °C

2: copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 130 °C / Microwave irradiation

3: dichloromethane / 4 h / 20 °C

With copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; Iodine monochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; 2: Sonogashira coupling;
DOI:10.1002/cmdc.201100522

Reference yield:

: 16114-53-7
4-iodo-3-methyl-5-phenylisoxazole

: 1368806-99-8
C₂HF₃O₂*C₁₇H₂₀N₂O

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 130 °C / Microwave irradiation

2: dichloromethane / 4 h / 20 °C

With copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; 1: Sonogashira coupling;
DOI:10.1002/cmdc.201100522

Reference yield:

: 536-74-3
phenylacetylene

: 1368806-99-8
C₂HF₃O₂*C₁₇H₂₀N₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 - 0 °C

1.2: 1 h / -78 - 20 °C

2.1: pyridine; hydroxylamine hydrochloride; sodium sulfate / 17 h / Reflux

3.1: Iodine monochloride / dichloromethane / 20 °C

4.1: copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 130 °C / Microwave irradiation

5.1: dichloromethane / 4 h / 20 °C

With pyridine; copper(l) iodide; n-butyllithium; bis(triphenylphosphine)palladium(II)-chloride; hydroxylamine hydrochloride; Iodine monochloride; sodium sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 4.1: Sonogashira coupling;
DOI:10.1002/cmdc.201100522