Technology Process of C28H35NO4
There total 9 articles about C28H35NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: pyridine / dichloromethane / 24 h
2: bromine / diethyl ether / 95 h / 5 °C
3: sodium azide / water; acetone / 20 °C
4: triphenylphosphine / 1,4-dioxane / 3 h / 75 °C
5: sodium hydroxide / ethanol / 2 h / 20 °C
6: triethylamine / dichloromethane / 1 h / 0 °C
7: potassium carbonate / acetonitrile / 24 h / Reflux
With
pyridine; sodium azide; bromine; potassium carbonate; triethylamine; triphenylphosphine; sodium hydroxide;
In
1,4-dioxane; diethyl ether; ethanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1246/cl.2012.406
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium azide / water; acetone / 20 °C
2: triphenylphosphine / 1,4-dioxane / 3 h / 75 °C
3: sodium hydroxide / ethanol / 2 h / 20 °C
4: triethylamine / dichloromethane / 1 h / 0 °C
5: potassium carbonate / acetonitrile / 24 h / Reflux
With
sodium azide; potassium carbonate; triethylamine; triphenylphosphine; sodium hydroxide;
In
1,4-dioxane; ethanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1246/cl.2012.406
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C
2: triethylamine / dichloromethane / 1 h / 0 °C
3: potassium carbonate / acetonitrile / 24 h / Reflux
With
sodium tetrahydroborate; potassium carbonate; triethylamine;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1246/cl.2012.406